三丁基(4-甲氧基苯基)锡合成路线 (共 91 条)
反应条件
triphenyl-arsane; lithium chloride; tris-(dibenzylideneacetone)dipalladium(0) in various solvent(s) T=80°C; 70 h;
参考文献
Farina, Vittorio; Krishnan, Bala; Marshall, Daniel R.; Roth, Gregory P.
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5434 - 5444
反应条件
Cu(I) 3-methylsalicylate in N,N-dimethyl-formamide 1 h; Microwave irradiationHeatingInert atmosphereSealed tube;
参考文献
Zhang, Zhihui; Lindale, Matthew G.; Liebeskind, Lanny S.
Journal of the American Chemical Society, 2011 , vol. 133, # 16 p. 6403 - 6410
反应条件
CsSO4F in chloroform; acetonitrile 72 h; Ambient temperature;
参考文献
Bryce, Martin R.; Chambers, Richard D.; Mullins, Stephen T.; Parkin, Ann
Bulletin de la Societe Chimique de France, 1986 , # 6 p. 930 - 932
反应条件
benzoylchlorobis(triphenylphosphine)palladium(II) in chloroform T=65°C; 5 h;
参考文献
Labadie, Jeff W.; Tueting, David; Stille, J. K.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4634 - 4642
反应条件
copper dichloride; palladium dichloride in acetic acid T=25°C; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 74, # 7 p. 1343 - 1348
反应条件
2,6-di-tert-butyl-4-methyl-phenol; 4 A molecular sieve; lithium chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in N,N-dimethyl-formamide T=90°C; P=760 Torr; 13 h;
参考文献
Echavarren,A.M.; Stille,J.K.
Journal of the American Chemical Society, 1988 , vol. 110, p. 1557
反应条件
LiCl; CO; dichloro{1,1'-bis(diphenylphosphino)ferrocene}palladium(II) in N,N-dimethyl-formamide the triflate and the stannane in DMF contg. the Pd catalyst and LiCl heated at 90°C under 1 atm CO for 13 h; cooled to room temp., dild. with ether, filtered, filtrate washed with water and satd. NaCl soln., dried, concd., chromd. (flash column, hexanes/EtOAc);
参考文献
Echavarren,A.M.; Stille,J.K.
Journal of the American Chemical Society, 1988 , vol. 110, p. 1557
反应条件
Pd/Fe3O4; cesium fluoride in 1,4-dioxane T=100°C; Stille Cross Coupling; 18 h;
参考文献
Bulletin of the Korean Chemical Society, , vol. 33, # 8 p. 2789 - 2792
反应条件
triphenyl-arsane; lithium chloride; tris-(dibenzylideneacetone)dipalladium(0) in various solvent(s) T=80°C; 70 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 20 p. 5434 - 5444
反应条件
CuDPP in N,N-dimethyl-formamide T=60°C; 12 h; Inert atmosphere;
参考文献
Zhang, Zhihui; Yu, Ying; Liebeskind, Lanny S.
Organic Letters, 2008 , vol. 10, # 14 p. 3005 - 3008