9-(2-羟乙基)腺嘌呤合成路线 (共 23 条)
反应条件
thionyl bromide
0.333333 h; Ambient temperature;
参考文献
Shimidzu, Takeo; Kanou, Takeshi; Murakami, Akira; Yamana, Kazushige; Inagaki, Hiroshi; Donkai, Nobuo
Journal of Chemical Research, Miniprint, 1980 , # 11 p. 4668 - 4693
反应条件
1.1: sodium tert-butoxide / dimethylformamide / 0.67 h / 20 °C
1.2: 27 percent / dimethylformamide / 72 h / 20 °C
2.1: 78 percent / TMSCl; LiAlH4 / tetrahydrofuran / -50 - 20 °C
View Scheme
参考文献
Barral, Karine; Priet, Stephane; Sire, Josephine; Neyts, Johan; Balzarini, Jan; Canard, Bruno; Alvarez, Karine
Journal of Medicinal Chemistry, 2006 , vol. 49, # 26 p. 7799 - 7806
反应条件
bromine in water
Ambient temperaturestoppered flask;
参考文献
Holy, Antonin; Kohoutova, Jitka; Merta, Ales; Votruba, Ivan
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 2 p. 459 - 477