2,2-二氧代-1,3-二氢苯并[c]噻吩-5-胺合成路线 （共 4 条）
反应条件
hydrogenchloride; tin in ethanol
8 h; Heating;
参考文献
Tashbaev
Russian Chemical Bulletin, 2005 , vol. 54, # 2 p. 437 - 440
反应条件
1: 89.5 percent / acetic acid; H2O2 / 4 h / 20 - 95 °C
2: 81.2 percent / nitric acid; acetic acid; Ac2O / 5 h / 10 °C
3: 81.4 percent / tin; hydrochloric acid / ethanol / 8 h / Heating
View Scheme
参考文献
Tashbaev
Russian Chemical Bulletin, 2005 , vol. 54, # 2 p. 437 - 440
反应条件
1: 81.2 percent / nitric acid; acetic acid; Ac2O / 5 h / 10 °C
2: 81.4 percent / tin; hydrochloric acid / ethanol / 8 h / Heating
View Scheme
参考文献
Tashbaev
Russian Chemical Bulletin, 2005 , vol. 54, # 2 p. 437 - 440
反应条件
1: 66.1 percent / sodium sulfide nonahydrate; benzyltriethylammonium chloride / benzene; H2O / 30 h / 20 °C
2: 89.5 percent / acetic acid; H2O2 / 4 h / 20 - 95 °C
3: 81.2 percent / nitric acid; acetic acid; Ac2O / 5 h / 10 °C
4: 81.4 percent / tin; hydrochloric acid / ethanol / 8 h / Heating
View Scheme
参考文献
Tashbaev
Russian Chemical Bulletin, 2005 , vol. 54, # 2 p. 437 - 440
