反,反,顺-1,5,9-环十二烷基三烯合成路线 (共 58 条)
反应条件
diethylaluminium chloride; titanium tetrachloride in benzene T=60°C; 8 h; Further byproducts given;
参考文献
Tetrahedron, , vol. 40, # 17 p. 3295 - 3302
反应条件
(η6-C6H6)Ti(AlCl4)2; alkali chloride T=50 - 100°C; P=1E-05 Torr; C6H6Ti(AlBr4)2 and other alkali halogenides; Rate constantProduct distribution;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 54, # 7 p. 1839 - 1845
反应条件
copper in diethyl ether T=180°C; 1) 20 Torr 2) 1 Torr;
参考文献
Tetrahedron, , vol. 42, # 6 p. 1711 - 1720
反应条件
tetrakis(cyclohexyloxo)titanium(IV); (Et)3Al2Cl3 in toluene T=50°C; 1 h; Other catalytic system (R = n-C3H7,iso-C3H7,n-C4H9,tert-c4H9,sec-C4H9,M-CH3C6H4), different ratio of catalysts, 60 deg C; Product distribution;
参考文献
Tsvetkov, V. F.; Likhomanenko, V. A.; Pisareva, V. S.; Korzhova, N. V.; Kazantsev, V. M.; et al
J. Appl. Chem. USSR (Engl. Transl.), 1983 , vol. 56, # 4 p. 1103 - 1107,1036 - 1039
反应条件
diethylaluminium chloride; titanium tetrachloride in benzene T=60°C; 6 h; in a sealed ampoule; Yield given;
参考文献
Journal of Organometallic Chemistry, , vol. 289, p. 331 - 340
反应条件
diethylaluminium chloride; titanium tetrachloride Further byproducts given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 15 p. 805 - 806
反应条件
diethylaluminium chloride; titanium tetrachloride; benzene T=40°C;
参考文献
Angewandte Chemie, , vol. 69, p. 397
Journal of Polymer Science, , vol. 38, p. 45
Makromolekulare Chemie, , vol. 69, p. 18,29,30,34
反应条件
titanium(II) bromoaluminate in benzene 1 h; high vacuum, other reagent;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 51, # 12 p. 2751 - 2759