反-4-氯-β-硝基苯乙烯合成路线 （共 30 条）
反应条件
acetic acid; benzylamine T=78 - 80°C; 3.5 h; Product distribution / selectivity;
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED
Patent: US2011/152572 A1, 2011 ;
Location in patent: Page/Page column 4-5 ;
反应条件
N-(chloromethylene)-N-methylmethanaminium chloride; sodium nitrite in neat (no solvent) T=100°C; P=1500.15 Torr; Microwave irradiation; Reagent/catalystTemperature;
参考文献
Kumar, M. Satish; Rajanna; Reddy, K. Rajendar; Venkateswarlu; Venkanna
Synthetic Communications, 2013 , vol. 43, # 19 p. 2672 - 2677
反应条件
C28H52N6O4 T=50°C; 48 h;
参考文献
Journal of the American Chemical Society, , vol. 131, # 32 p. 11478 - 11484
反应条件
ammonium nitrate in solid T=100 - 110°C; 0.05 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 39, # 23 p. 3977 - 3980
反应条件
mesoporous silica nanoparticles-NNH2-SO3H T=90°C; nitroaldol Henry reaction; 6 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 15, # 29 p. 7052 - 7062
反应条件
nitrogen(IV) oxide; ozone in dichloromethane T=-20°C; multistep reaction; other temperatures, reaction time, reagents; Product distribution;
参考文献
Suzuki, Hitomi; Mori, Tadashi
Journal of Organic Chemistry, 1997 , vol. 62, # 19 p. 6498 - 6502
反应条件
H-Y (SiO2/Al2O3 = 5.6) zeolite T=60°C; Aza-Henry reaction; 9 h;
参考文献
Applied Catalysis A: General, , vol. 388, # 1-2 p. 211 - 215
反应条件
triethylamine; trifluoroacetic anhydride T=0 - 20°C; 3 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 135, # 23 p. 8504 - 8507
反应条件
1: potassium tert-butylate / tetrahydrofuran; tert-butyl alcohol / 13 h / 0 - 20 °C / |Inert atmosphere 2: trifluoroacetic anhydride; triethylamine / 3 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 23 p. 8504 - 8507
反应条件
yolk–shell nanoparticles with basic (-NH2) core and acidic (-SO3H) shell T=90°C; 22 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 36 p. 9164 - 9168
