2,4-二苄氧基嘧啶-5-硼酸合成路线 (共 2 条)
反应条件
1: With n-butyllithium; tri-isopropoxy-borane in tetrahydrofuran; hexane; toluene T=20°C; 18 h; 2: With hydrogenchloride in tetrahydrofuran; hexane; toluene
参考文献
Seley, Katherine L.; Salim, Samer; Zhang, Liang; O'Daniel, Peter I.
Journal of Organic Chemistry, 2005 , vol. 70, # 5 p. 1612 - 1619
反应条件
1.1: 91 percent / NaH / various solvent(s); toluene / 18 h / 20 °C 2.1: n-butyllithium; B(OiPr)3 / hexane; tetrahydrofuran; toluene / 18 h / 20 °C 2.2: 95 percent / aq.HCl / toluene; tetrahydrofuran; hexane View Scheme
参考文献
Journal of Organic Chemistry, , vol. 70, # 5 p. 1612 - 1619