1-氯甲基-3-三氟甲基苯合成路线 （共 50 条）
参考文献
Helvetica Chimica Acta, , vol. 54, p. 868 - 897
Journal of Organic Chemistry, , vol. 42, # 5 p. 868 - 871
反应条件
1: NaBH4 / methanol / Ambient temperature 2: SOCl2 / toluene / 0.08 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 42, # 6 p. 1007 - 1017
反应条件
1: LiAlH4 2: SOCl2 View Scheme
参考文献
Helvetica Chimica Acta, , vol. 54, p. 868 - 897
Journal of Organic Chemistry, , vol. 42, # 5 p. 868 - 871
反应条件
1: aq. KI / methanol 2: NaOH / ethanol 3: LiAlH4 / diethyl ether View Scheme
参考文献
Lambert,J.B. et al.
Journal of the American Chemical Society, 1977 , vol. 99, # 9 p. 3059 - 3067
反应条件
hydrazine hydrate in ethanol 1.5 h; Reflux;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 60, # 44 p. 10942 - 10951
反应条件
1: Na2CO3; H2O 2: hydrogen; carbon monoxide; benzene / 190 °C / weitere Reagensien: Octacarbonyldikobalt u. Kobalt(II)-carbonat View Scheme
参考文献
Wender et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4079,4082
反应条件
water; sodium carbonate
参考文献
Wender et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4079,4082
反应条件
in acetonitrile Irradiation254 nm; Quantum yield;
参考文献
Cristol, Stanley J.; Bindel, Thomas H.
Journal of Organic Chemistry, 1980 , vol. 45, # 6 p. 951 - 957
反应条件
acetone 42 h; Irradiation300 nm; Quantum yield;
参考文献
Cristol, Stanley J.; Bindel, Thomas H.
Journal of Organic Chemistry, 1980 , vol. 45, # 6 p. 951 - 957
反应条件
1: carbon monoxide With C28H22CoN4O6 in butan-1-ol T=60°C; P=760.051 Torr; 2 h; GloveboxHigh pressureGreen chemistry; 2: 3-(trifluoromethyl)-benzyl chloride With tetra-(n-butyl)ammonium iodide; sodium hydroxide in butan-1-ol T=60°C; P=760.051 Torr; 22 h; GloveboxHigh pressureGreen chemistry; regioselective reaction;
参考文献
She, Meng-Yao; Xiao, Da-Wei; Yin, Bing; Yang, Zheng; Liu, Ping; Li, Jian-Li; Shi, Zhen
Tetrahedron, 2013 , vol. 69, # 35 p. 7264 - 7268
