3,4,5-三(苄氧基)苯甲酸甲酯合成路线 （共 14 条）
反应条件
1: water; sodium hydroxide / methanol / 1 h / Reflux
2: pyridine; thionyl chloride / benzene / 1.5 h / Reflux
3: pyridine; 4-(N,N-dimethlyamino)pyridine / chloroform / 5 h / Inert atmosphere
View Scheme
参考文献
Lee, Yong-Gyun; Song, Ju-Hyun; Lee, Eon-Jin; Lee, Do-Hun; Jung, Dai-Il; Hahn, Jung-Tai
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 6 p. 2051 - 2054
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 25°C; 2 h; Inert atmosphere;
参考文献
Percec, Virgil; Sun, Hao-Jan; Leowanawat, Pawaret; Peterca, Mihai; Graf, Robert; Spiess, Hans W.; Zeng, Xiangbing; Ungar, Goran; Heiney, Paul A.
Journal of the American Chemical Society, 2013 , vol. 135, # 10 p. 4129 - 4148
反应条件
1: lithium aluminium hydride / tetrahydrofuran / 2 h / Heating
2: thionyl chloride
View Scheme
参考文献
Rajamalli; Prasad, Edamana
Organic Letters, 2011 , vol. 13, # 14 p. 3714 - 3717
反应条件
1: LiAlH4 / tetrahydrofuran / 30 °C
2: 90 percent / pyridinium chlorochromate / CH2Cl2 / 1 h
View Scheme
参考文献
Zaveri, Nurulain T.
Organic Letters, 2001 , vol. 3, # 6 p. 843 - 845
