in dichloromethane byproducts: Me2SO; (N2); std. Schlenk technique; Pt complex was reacted with P ligand in CH2Cl2; mixt. was set aside for few h; evapd.; petroleum ether added; cooled; crystd.;
in benzene
addn. of DMSO to Pt complex soln.; reducing volume after 2h; pptn.; storing overnight in a vac. desiccator under reduced pressure; crystn.; filtration; washing (ether); drying (vac.); elem. anal.;
参考文献
Appleton, Trevor G.; Hall, John R.; Williams, Mark A.
Journal of Organometallic Chemistry, 1986 , vol. 303, p. 139 - 150
Eaborn, Colin; Kundu, Kalipada; Pidcock, Alan
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1981 , p. 933 - 938
Eaborn, Colin; Kundu, Kalipada; Pidcock, Alan
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1981 , p. 933 - 938
