2,2-二氟-1-(4-甲基苯基)-乙酮合成路线 （共 8 条）
反应条件
1: flash-vacuum pyrolysis;
2: With water
参考文献
Boonkitpattarakul, Kanhokthron; Soorukram, Darunee; Tuchinda, Patoomratana; Reutrakul, Vichai; Pohmakotr, Manat
Journal of Fluorine Chemistry, 2011 , vol. 132, # 11 p. 987 - 990
参考文献
Kirij, Nataliya V.; Babadzhanova, Lesya A.; Movchun, Valeria N.; Yagupolskii, Yurii L.; Tyrra, Wieland; Naumann, Dieter; Fischer, Hendrik T.M.; Scherer, Harald
Journal of Fluorine Chemistry, 2008 , vol. 129, # 1 p. 14 - 21
反应条件
hydrogenchloride
T=20°C;
参考文献
Surya Prakash; Hu; Olah
Journal of Fluorine Chemistry, 2001 , vol. 112, # 2 p. 357 - 362
反应条件
1: Mg / tetrahydrofuran / 2 h / 0 °C
2: 0.73 g / aq. HCl / 20 °C
View Scheme
参考文献
Surya Prakash; Hu; Olah
Journal of Fluorine Chemistry, 2001 , vol. 112, # 2 p. 357 - 362
反应条件
hydrogenchloride; sodium carbonate; N-fluorobislt;(trifluoromethyl)sulfonylgt;imide
1.) CH2Cl2, room temp., 5 h, 2.) CH2Cl2; Yield given. Multistep reaction;
参考文献
Ying; DesMarteau; Gotoh
Tetrahedron, 1996 , vol. 52, # 1 p. 15 - 22
反应条件
hydrogenchloride; sodium carbonate; N-fluorobislt;(trifluoromethyl)sulfonylgt;imide
1.) CH2Cl2, room temp., 5 h, 2.) CH2Cl2; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ying; DesMarteau; Gotoh
Tetrahedron, 1996 , vol. 52, # 1 p. 15 - 22
参考文献
Kazennikova,G.V. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1961 , p. 985 - 988
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , # 6 p. 1066 - 1069
反应条件
1: NaBH4 / dioxane; H2O
3: H2 / Pd-C / ethanol / Ambient temperature
View Scheme
参考文献
DePuy,C.H.; Schultz,A.L.
Journal of Organic Chemistry, 1974 , vol. 39, # 7 p. 878 - 881
