[(3-丁烯-1-基氧基)甲基]苯合成路线 (共 32 条)
反应条件
1: O3, t-BuNH2*BH3 2: CBr4, PPh3 View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 1 p. 133 - 136
反应条件
1: With dimethylsulfide borane complex in tetrahydrofuran T=20°C; 4 h; 2: With benzene-1,2-diol; triethylamine in tetrahydrofuran T=20°C; 2.5 h; 3: With oxygen in tetrahydrofuran T=20°C; 12 h;
参考文献
Cadot, Christine; Dalko, Peter I.; Cossy, Janine; Ollivier, Cyril; Chuard, Rachel; Renaud, Philippe
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7193 - 7202
参考文献
Dolle, Roland E.; McNair, David
Tetrahedron Letters, 1993 , vol. 34, # 1 p. 133 - 136
反应条件
1: titanium(IV) isopropylate With n-butyllithium in tetrahydrofuran T=0°C; 0.0833333 h; Inert atmosphere; 2: ((but-3-en-1-yloxy)methyl)benzene in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 3: carbon dioxide in tetrahydrofuran T=0°C; 0.333333 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 70, # 4 p. 787 - 794
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium perchlorate; palladium diacetate in water; acetonitrile T=20°C; Electrochemical reaction;
参考文献
Mitsudo, Koichi; Kaide, Takashi; Nakamoto, Eriko; Yoshida, Kenta; Tanaka, Hideo
Journal of the American Chemical Society, 2007 , vol. 129, # 8 p. 2246 - 2247
反应条件
oxygen; 1-n-butyl-3-methylimidazolium tetrafluoroborate; copper(l) chloride; palladium dichloride in water T=60°C; Wacker oxidation; 25 h;
参考文献
Ansari; Joyasawal, Sipak; Gupta, Manoj K.; Yadav; Gree
Tetrahedron Letters, 2005 , vol. 46, # 44 p. 7507 - 7510
反应条件
hydrogen; TMSB; palladium in ethanol T=20°C; P=760 Torr; 40 h;
参考文献
Belotti, Damien; Cantagrel, Guillaume; Combellas, Catherine; Cossy, Janine; Kanoufi, Frederic; Nunige, Sandra
New Journal of Chemistry, 2005 , vol. 29, # 6 p. 761 - 764
反应条件
4-(picolyloxy)-1-butene; hydrogen; (.eta.4-1,5-cyclooctadiene)(pyridine)(tricyclohexylphosphine)iridium(I) hexafluorophosphate in methanol P=760 Torr; 17 h; Ambient temperature;
参考文献
Westwell, Andrew D.; Williams, Jonathan M. J.
Tetrahedron, 1997 , vol. 53, # 38 p. 13063 - 13078
反应条件
in benzene 11 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Penn, John H.; Zhu, Chen; Deng, Dao-Li; Petersen, Jeffrey L.
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 3037 - 3039
反应条件
1: titanium(IV) isopropylate With n-butyllithium in tetrahydrofuran T=0°C; 0.0833333 h; Inert atmosphere; 2: ((but-3-en-1-yloxy)methyl)benzene in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 3: carbon dioxide in tetrahydrofuran T=0°C; 0.333333 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 70, # 4 p. 787 - 794