2,3,6,7,10,11-六(己氧基)苯并菲合成路线 （共 17 条）
反应条件
9-BrBBN in dichloromethane T=0°C; 38 h;
参考文献
Allen; Diele; Harris; Hegmann; Kariuki; Lose; Preece; Tschierske
Journal of Materials Chemistry, 2001 , vol. 11, # 2 p. 302 - 311
反应条件
anhydrous iron chloride in nitromethane; dichloromethane
T=0°C; 3 h;
参考文献
Kong, Xiangfei; He, Zhiqun; Gopee, Hemant; Jing, Xiping; Cammidge, Andrew N.
Tetrahedron Letters, 2011 , vol. 52, # 1 p. 77 - 79
反应条件
[MoCl5] in dichloromethane
0.333333 h; Ambient temperature;
参考文献
Kumar, Sandeep; Manickam
Chemical Communications, 1997 , # 17 p. 1615 - 1616
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in toluene
T=150°C; 0.666667 h; Inert atmosphereMicrowave irradiation;
参考文献
Zhao, Baomin; Liu, Bo; Png, Rui Qi; Zhang, Kai; Lim, Kheng Aik; Luo, Jing; Shao, Jinjun; Ho, Peter K.H.; Chi, Chunyan; Wu, Jishan
Chemistry of Materials, 2010 , vol. 22, # 2 p. 435 - 449
反应条件
anhydrous iron chloride; sulfuric acid in dichloromethane
T=20°C; 1 h;
参考文献
Yelamaggad, Channabasaveshwar V.; Achalkumar, Ammathnadu S.; Rao, D. S. Shankar; Nobusawa, Mitsunori; Akutsu, Hiroki; Yamada, Jun-Ichi; Nakatsuji, Shin'Ichi
Journal of Materials Chemistry, 2008 , vol. 18, # 29 p. 3433 - 3437
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=80°C;
参考文献
Chiang, Long Y.; Safinya, C. R.; Clark, N. A.; Liang, K. S.; Bloch, A. N.
Journal of the Chemical Society, Chemical Communications, 1985 , # 11 p. 695 - 696
反应条件
1.1: potassium carbonate; potassium iodide / acetone / 48 h / 65 °C / Inert atmosphere
2.1: N-bromosuccinmide / tetrahydrofuran / Darkness
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 20 °C
3.2: 24 h / -78 - 20 °C
4.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / toluene / 0.67 h / 150 °C / Inert atmosphere; Microwave irradiation
View Scheme
参考文献
Zhao, Baomin; Liu, Bo; Png, Rui Qi; Zhang, Kai; Lim, Kheng Aik; Luo, Jing; Shao, Jinjun; Ho, Peter K.H.; Chi, Chunyan; Wu, Jishan
Chemistry of Materials, 2010 , vol. 22, # 2 p. 435 - 449
反应条件
1.1: potassium carbonate; potassium iodide / acetone / 48 h / 65 °C / Inert atmosphere
2.1: N-bromosuccinmide / tetrahydrofuran / Darkness
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 20 °C
3.2: 24 h / -78 - 20 °C
4.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / toluene / 0.67 h / 150 °C / Inert atmosphere; Microwave irradiation
View Scheme
参考文献
Zhao, Baomin; Liu, Bo; Png, Rui Qi; Zhang, Kai; Lim, Kheng Aik; Luo, Jing; Shao, Jinjun; Ho, Peter K.H.; Chi, Chunyan; Wu, Jishan
Chemistry of Materials, 2010 , vol. 22, # 2 p. 435 - 449
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 20 °C
1.2: 24 h / -78 - 20 °C
2.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / toluene / 0.67 h / 150 °C / Inert atmosphere; Microwave irradiation
View Scheme
参考文献
Zhao, Baomin; Liu, Bo; Png, Rui Qi; Zhang, Kai; Lim, Kheng Aik; Luo, Jing; Shao, Jinjun; Ho, Peter K.H.; Chi, Chunyan; Wu, Jishan
Chemistry of Materials, 2010 , vol. 22, # 2 p. 435 - 449
反应条件
iron(III) chloride in dichloromethane
1 h; Ambient temperature;
参考文献
Boden, Neville; Bushby, Richard J.; Cammidge, Andrew N.
Journal of the Chemical Society, Chemical Communications, 1994 , # 4 p. 465 - 466
