3-(3,4,5-三甲氧基苯基)丙酸乙酯合成路线 （共 13 条）
反应条件
formic acid; triethylamine in ethanol
反应条件
sodium chloride in dimethyl sulfoxide 5 h; Reflux;
参考文献
Zheng, Cheng; Guo, Yibing; Meng, Ying; Dou, Sufeng; Shao, Jian; Yang, Yumin
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 5 p. 654 - 664
反应条件
hydrogen; palladium on activated charcoal in ethanol Yield given;
参考文献
European Journal of Medicinal Chemistry, , vol. 23, # 1 p. 53 - 62
反应条件
1: 1) piperidine, 2) conc. H2SO4 / 1) pyridine 2: hydrogen / 5percent Pd/C / ethanol View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 23, # 1 p. 53 - 62
反应条件
Pd-BaSO4; acetic acid T=100°C; Hydrogenation;
参考文献
DE545853 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 2867
反应条件
1: thionyl chloride / dichloromethane 2: potassium carbonate / dimethyl sulfoxide / 6 h / 50 °C 3: sodium chloride / dimethyl sulfoxide / 5 h / |Reflux View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 52, # 5 p. 654 - 664
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran 2: thionyl chloride / dichloromethane 3: potassium carbonate / dimethyl sulfoxide / 6 h / 50 °C 4: sodium chloride / dimethyl sulfoxide / 5 h / |Reflux View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 52, # 5 p. 654 - 664
反应条件
1: potassium carbonate / dimethyl sulfoxide / 6 h / 50 °C 2: sodium chloride / dimethyl sulfoxide / 5 h / |Reflux View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 52, # 5 p. 654 - 664
参考文献
Koo
Journal of the American Chemical Society, 1953 , vol. 75, p. 1889
反应条件
1: sodium wire / diethyl ether / 18 h / Ambient temperature
2: ethanol / 7 h / Heating
3: 90 percent / aq. NaOH / ethanol / 60 °C
4: 38 percent / 5 h / 140 - 150 °C
View Scheme
参考文献
Brown; Blakemore; Durant; Emmett; Ganellin; Parsons; Rawlings; Walker
European Journal of Medicinal Chemistry, 1988 , vol. 23, # 1 p. 53 - 62
