4-(3-甲基苯基)吗啉合成路线 （共 23 条）
反应条件
potassium tert-butylate in dimethyl sulfoxide
0.0833333 h; Heatingmicrowave irradiation;
参考文献
Shi, Lei; Wang, Min; Fan, Chun-An; Zhang, Fu-Min; Tu, Yong-Qiang
Organic Letters, 2003 , vol. 5, # 19 p. 3515 - 3517
反应条件
pyridine; copper diacetate; 4 A molecular sieve in 1,4-dioxane
T=20°C; Arylation; 48 h;
参考文献
Lam, Patrick Y.S.; Clark, Charles G.; Saubern, Simon; Adams, Jessica; Averill, Kristin M.; Chan, Dominic M. T.; Combs, Andrew
Synlett, 2000 , # 5 p. 674 - 676
反应条件
bicyclo-[2.2.1]hept-2-ene; tris(4-methoxyphenyl)-phosphine; palladium diacetate; caesium carbonate; isopropyl alcohol in toluene
T=100°C; 24 h; Inert atmosphereSealed tube; Reagent/catalystpH-valueConcentration;
参考文献
Dong, Zhe; Dong, Guangbin
Journal of the American Chemical Society, 2013 , vol. 135, # 49 p. 18350 - 18353
反应条件
cesium hydroxide in dimethyl sulfoxide
T=20°C; 0.166667 h;
参考文献
Varala, Ravi; Ramu; Alam, M. Mujahid; Adapa, Srinivas R.
Synlett, 2004 , # 10 p. 1747 - 1750
反应条件
iron(III) oxide; L-proline; sodium t-butanolate in dimethyl sulfoxide
T=135°C; 24 h;
参考文献
Quo, Diliang; Huang, He; Xu, Jinyi; Jiang, Hualiang; Liu, Hong
Organic Letters, 2008 , vol. 10, # 20 p. 4513 - 4516
反应条件
iron(III) oxide; copper acetylacetonate; caesium carbonate in water; dimethyl sulfoxide
T=150°C; 0.5 h; sealed vialMicrowave irradiation;
参考文献
Guo, Diliang; Huang, He; Zhou, Yu; Xu, Jinyi; Jiang, Hualiang; Chen, Kaixian; Liu, Hong
Green Chemistry, 2010 , vol. 12, # 2 p. 276 - 281
反应条件
1: triethylamine / tetrachloromethane / 0 - 20 °C / Inert atmosphere
2: NiCl(1-naphthyl)(PPh3)2; sodium hydride; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride / 1,4-dioxane / 0.5 h / 110 °C / Inert atmosphere
View Scheme
参考文献
Huang, Jin-Hua; Yang, Lian-Ming
Organic Letters, 2011 , vol. 13, # 14 p. 3750 - 3753
反应条件
potassium hexamethylsilazane in 1,4-dioxane
T=100°C; metal-free Buchwald-Hartwig amination; 0.25 h; Inert atmosphere;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Tetrahedron, 2009 , vol. 65, # 6 p. 1180 - 1187
反应条件
potassium hexamethylsilazane in 1,4-dioxane
T=100°C; metal-free Buchwald-Hartwig amination; 0.25 h; Inert atmosphere;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Tetrahedron, 2009 , vol. 65, # 6 p. 1180 - 1187
反应条件
potassium tert-butylate in dimethyl sulfoxide
0.0833333 h; Heatingmicrowave irradiation;
参考文献
Shi, Lei; Wang, Min; Fan, Chun-An; Zhang, Fu-Min; Tu, Yong-Qiang
Organic Letters, 2003 , vol. 5, # 19 p. 3515 - 3517
