4-(3-甲基苯基)吗啉合成路线 （共 23 条）
反应条件
Ni(PPh3)2(1-naphthyl)Cl; potassium tert-butylate; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in toluene
T=23°C; 24 h; Inert atmosphere;
参考文献
Fan, Xin-Heng; Li, Gang; Yang, Lian-Ming
Journal of Organometallic Chemistry, 2011 , vol. 696, # 13 p. 2482 - 2484
反应条件
[NiCl2(1,2-dimethoxyethane)]; 4,4,5,5-tetramethyl-2-phenyl-[1,3,2]-dioxaborolane; sodium t-butanolate; SIDip*HCl in 1,4-dioxane
T=23 - 80°C; 4 h; Inert atmosphere;
参考文献
Hie, Liana; Ramgren, Stephen D.; Mesganaw, Tehetena; Garg, Neil K.
Organic Letters, 2012 , vol. 14, # 16 p. 4182 - 4185
反应条件
[NiCl2(1,2-dimethoxyethane)]; 4,4,5,5-tetramethyl-2-phenyl-[1,3,2]-dioxaborolane; sodium t-butanolate; SIDip*HCl in 1,4-dioxane
T=23 - 80°C; 4 h; Inert atmosphere;
参考文献
Hie, Liana; Ramgren, Stephen D.; Mesganaw, Tehetena; Garg, Neil K.
Organic Letters, 2012 , vol. 14, # 16 p. 4182 - 4185
反应条件
copper acetylacetonate; oxygen; benzoic acid in acetonitrile
T=50°C; 12 h;
参考文献
Zhou, Yanping; Xie, Yinjun; Yang, Lei; Xie, Pan; Huang, Hanmin
Tetrahedron Letters, 2013 , vol. 54, # 21 p. 2713 - 2716
反应条件
NiCl(1-naphthyl)(PPh3)2; sodium hydride; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in 1,4-dioxane
T=110°C; Inert atmosphere;
参考文献
Huang, Jin-Hua; Yang, Lian-Ming
Organic Letters, 2011 , vol. 13, # 14 p. 3750 - 3753
反应条件
NHC-Pd(II)-Im; potassium tert-butylate in tetrahydrofuran
T=20°C; 6 h; Inert atmosphere;
参考文献
Chen, Wen-Xin; Shao, Li-Xiong
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9236 - 9239,4
Title/Abstract Show Details
Chen, Wen-Xin; Shao, Li-Xiong
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9236 - 9239
反应条件
NiCl(1-naphthyl)(PPh3)2; sodium hydride; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in 1,4-dioxane
T=110°C; 0.5 h; Inert atmosphere;
参考文献
Huang, Jin-Hua; Yang, Lian-Ming
Organic Letters, 2011 , vol. 13, # 14 p. 3750 - 3753
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; n-butyllithium; lithium tert-butylate; Ni(II)/C in toluene
10 h; Heating;
参考文献
Tasler, Stefan; Lipshutz, Bruce H.
Journal of Organic Chemistry, 2003 , vol. 68, # 4 p. 1190 - 1199
反应条件
palladium 10 on activated carbon; sodium t-butanolate; 2-dicyclohexylphosphino-1,1'-biphenyl in tert-butyl alcohol
T=100°C; Buchwald-Hartwig amination; Inert atmosphere;
参考文献
Komaromi, Anna; Novak, Zoltan
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 9 p. 1523 - 1532
反应条件
[Ru(II)(η6-benzene)(μ-Cl)Cl]2; silver trifluoromethanesulfonate; tris(p-fluoro phenyl)phosphine in 1,4-dioxane
24 h; Inert atmosphereMolecular sieveReflux;
参考文献
Otsuka, Maiko; Yokoyama, Hiroya; Endo, Kohei; Shibata, Takanori
Synlett, 2010 , # 17 p. 2601 - 2606
