4-(三氟甲基硫基)苯乙腈合成路线 (共 6 条)
反应条件
1: 2-(4-bromophenyl)ethanenitrile With Pd(CH2SiMe3)2(cod); cyclohexyl BrettPhos in toluene T=80°C; 0.0166667 h; Inert atmosphere; 2: silver (I) trifluoro methyl sulfide With Ph(Et)3NI in toluene T=80°C; 2 h; Inert atmosphere;
参考文献
Teverovskiy, Georgiy; Surry, David S.; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 32 p. 7312 - 7314
反应条件
in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; dimethyl sulfoxide
反应条件
[Ni0(1,5-cyclooctadiene)2]; 4,4'-dimethoxy-2,2'-bipyridine in tetrahydrofuran T=20°C; 22 h; Inert atmosphere;
参考文献
Zhang, Cheng-Pan; Vicic, David A.
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 183 - 185
反应条件
1: Br2 / benzene / Irradiation 2: ethanol View Scheme
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 35, p. 1628 - 1636,1631 - 1637
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 35, p. 1628 - 1636,1631 - 1637
参考文献
Orda,V.V. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1965 , vol. 35, p. 1628 - 1636,1631 - 1637