4-甲氧基苯甲酰基氟化物合成路线 （共 32 条）
反应条件
water T=25°C; also with D2O, effect of salts; Rate constant;
参考文献
Song, Byeong Doo; Jencks, William P.
Journal of the American Chemical Society, 1989 , vol. 111, # 22 p. 8470 - 8479
反应条件
1: hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane / chlorobenzene / 3 h / Inert atmosphere; Reflux 2: hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; oxygen; 1,2-bis-(diphenylphosphino)ethane / chlorobenzene / 9 h / Air atmosphere; Reflux View Scheme
参考文献
Arisawa, Mieko; Igarashi, Yui; Kobayashi, Haruki; Yamada, Toru; Bando, Kentaro; Ichikawa, Takuya; Yamaguchi, Masahiko
Tetrahedron, 2011 , vol. 67, # 40 p. 7846 - 7859
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane in chlorobenzene
3 h; RefluxInert atmosphere;
参考文献
Arisawa, Mieko; Igarashi, Yui; Kobayashi, Haruki; Yamada, Toru; Bando, Kentaro; Ichikawa, Takuya; Yamaguchi, Masahiko
Tetrahedron, 2011 , vol. 67, # 40 p. 7846 - 7859
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; cis-DPPEthylene in chlorobenzene
3 h; Inert atmosphereReflux;
参考文献
Arisawa, Mieko; Igarashi, Yui; Kobayashi, Haruki; Yamada, Toru; Bando, Kentaro; Ichikawa, Takuya; Yamaguchi, Masahiko
Tetrahedron, 2011 , vol. 67, # 40 p. 7846 - 7859
反应条件
pyridine; hydrogen fluoride; dicyclohexyl-carbodiimide in dichloromethane
T=20°C; 3 h;
参考文献
Chen, Chinpiao; Chien, Chin-Tzu; Su, Chu-Hsiang
Journal of Fluorine Chemistry, 2002 , vol. 115, # 1 p. 75 - 77
反应条件
CsSO4F in acetonitrile
T=35°C; 1.5 h;
参考文献
Stavber, Stojan; Planinsek, Zdenka; Zupan, Marko
Journal of Organic Chemistry, 1992 , vol. 57, # 20 p. 5334 - 5337
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; cis-DPPEthylene in chlorobenzene
2 h; Inert atmosphereReflux;
参考文献
Arisawa, Mieko; Igarashi, Yui; Kobayashi, Haruki; Yamada, Toru; Bando, Kentaro; Ichikawa, Takuya; Yamaguchi, Masahiko
Tetrahedron, 2011 , vol. 67, # 40 p. 7846 - 7859
反应条件
potassium fluoride; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide
T=80°C; 20 h; Inert atmosphereSealed tube;
参考文献
Ueda, Tsuyoshi; Konishi, Hideyuki; Manabe, Kei
Organic Letters, 2013 , vol. 15, # 20 p. 5370 - 5373
反应条件
cesium fluoride; bis-triphenylphosphine-palladium(II) chloride in various solvent(s)
T=80°C; P=760 Torr; 16.5 h;
参考文献
Sakakura, Toshiyasu; Chaisupakitsin, Malinee; Hayashi, Teruyuki; Tanaka, Masato
Journal of Organometallic Chemistry, 1987 , vol. 334, p. 205 - 212
反应条件
tetrafluoroboric acid in dichloromethane
Fluorination; Decomposition; 4 h; Heating;
参考文献
Wagner, Ruediger; Wiedel, Bernd; Guenther, Wolfgang; Goerls, Helmar; Anders, Ernst
European Journal of Organic Chemistry, 1999 , # 9 p. 2383 - 2390
