4-重氮基-4H-咪唑-5-甲酰胺合成路线 (共 11 条)
反应条件
potassium carbonate 1.) water, ethyl acetate, 25 deg C, 18 h; 2.) ethyl acetate, 18 h; Yield given. Multistep reaction;
参考文献
Baig, Ghouse Unissa; Stevens, Malcolm F. G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 665 - 670
反应条件
hydrogenchloride in sodium hydroxide T=0 - 3°C; Cyclization; pH=3;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 33, # 9 p. 1086 - 1091
反应条件
17β-hydrazoestra-1,3,5(10)-trien-3-ol in ethanol; chloroform T=20°C;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 40, # 11 p. 1470 - 1476
反应条件
citric acid in water; dimethyl sulfoxide 10 h; Irradiationsunlight;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1433 - 1436
反应条件
in ethyl acetate T=30°C; 48 h;
参考文献
Stevens, Malcolm F. G.; Hickman, John A.; Stone, Robert; Gibson, Neil W.; Baig, Ghouse Unissa; et al.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 2 p. 196 - 201
反应条件
in dichloromethane T=25°C; 480 h;
参考文献
Journal of Medicinal Chemistry, , vol. 27, # 2 p. 196 - 201
反应条件
potassium carbonate 1.) water, ethyl acetate, 2 d; 2.) 24 h, ethyl acetate; Yield given. Multistep reaction;
参考文献
Baig, Ghouse Unissa; Stevens, Malcolm F. G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 665 - 670
反应条件
hydrogenchloride; sodium acetate; sodium nitrite
T=0°C;
参考文献
Baig, Ghouse Unissa; Stevens, Malcolm F. G.; Stone, Robert
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 8 p. 1811 - 1820
反应条件
hydrogenchloride; sodium acetate; sodium nitrite
T=0°C;
参考文献
Baig, Ghouse Unissa; Stevens, Malcolm F. G.; Stone, Robert
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 8 p. 1811 - 1820
反应条件
in ethanol
T=25°C; 12 h;
参考文献
Stevens, Malcolm F. G.; Hickman, John A.; Stone, Robert; Gibson, Neil W.; Baig, Ghouse Unissa; et al.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 2 p. 196 - 201