3,4-二溴-2,5-二甲基噻吩1,1-二氧化物合成路线 （共 4 条）
反应条件
boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid in dichloromethane
T=-20°C; 3 h;
参考文献
Thiemann, Thies; Ohira, Daisuke; Arima, Kazuya; Sawada, Tsuyoshi; Mataka, Shuntaro; Marken, Frank; Compton, Richard G.; Bull, Steven D.; Davies, Stephen G.
Journal of Physical Organic Chemistry, 2000 , vol. 13, # 10 p. 648 - 653
反应条件
aluminum oxide; iron (III) hydroxide; ethylenediaminetetraacetic acid; dihydrogen peroxide in methanol; water
T=50 - 55°C; 5 h; Mechanism;
参考文献
Nagieva
Russian Journal of Physical Chemistry A, 2009 , vol. 83, # 11 p. 1873 - 1878
反应条件
dihydrogen peroxide; acetic acid
参考文献
Melles; Backer
Recueil des Travaux Chimiques des Pays-Bas, 1953 , vol. 72, p. 314,321
反应条件
1: carbon disulfide; copper (I)-cyanide; bromine / Erwaermen des Reaktionsprodukts mit aethanol. Kalilauge
2: acetic acid; aqueous hydrogen peroxide
View Scheme
参考文献
Melles; Backer
Recueil des Travaux Chimiques des Pays-Bas, 1953 , vol. 72, p. 314,321
