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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
去铁胺
合成路线
（共 17 条）
112139-65-8
→
反应条件
70-51-9
去铁胺
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in methanol
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 11 p. 3182 - 3187
129245-21-2
(5-氨基戊基)(苯基甲氧基)氨基甲酸叔丁酯
→
反应条件
70-51-9
去铁胺
反应条件
1: 99 percent / diphenyl phosphorazidate, triethylamine / dimethylformamide / 17 h / 0 - 20 °C 2: 87 percent / trifluoroacetic acid (TFA) / CH2Cl2 / 0.75 h / 0 - 20 °C 3: 96 percent / pyridine 4: 95 percent / diphenyl phosphorazidate, triethylamine / dimethylformamide / 17 h / 0 - 20 °C 5: 100 percent / trifluoroacetic acid (TFA) / CH2Cl2 6: 91 percent / pyridine / 12 h 7: H2, HCl / 10percent Pd/C / methanol View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 11 p. 3182 - 3187
129245-24-5
→
反应条件
70-51-9
去铁胺
反应条件
1: 95 percent / diphenyl phosphorazidate, triethylamine / dimethylformamide / 17 h / 0 - 20 °C 2: 100 percent / trifluoroacetic acid (TFA) / CH2Cl2 3: 91 percent / pyridine / 12 h 4: H2, HCl / 10percent Pd/C / methanol View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 11 p. 3182 - 3187
130946-41-7
→
反应条件
70-51-9
去铁胺
反应条件
1: 91 percent / pyridine / 12 h 2: H2, HCl / 10percent Pd/C / methanol View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 11 p. 3182 - 3187
130946-40-6
→
反应条件
70-51-9
去铁胺
反应条件
1: 100 percent / trifluoroacetic acid (TFA) / CH2Cl2 2: 91 percent / pyridine / 12 h 3: H2, HCl / 10percent Pd/C / methanol View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 11 p. 3182 - 3187
112139-60-3
→
反应条件
70-51-9
去铁胺
反应条件
1: 99 percent / diphenyl phosphorazidate, triethylamine / dimethylformamide / 17 h / 0 - 20 °C 2: 87 percent / trifluoroacetic acid (TFA) / CH2Cl2 / 0.75 h / 0 - 20 °C 3: 96 percent / pyridine 4: 95 percent / diphenyl phosphorazidate, triethylamine / dimethylformamide / 17 h / 0 - 20 °C 5: 100 percent / trifluoroacetic acid (TFA) / CH2Cl2 6: 91 percent / pyridine / 12 h 7: H2, HCl / 10percent Pd/C / methanol View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 11 p. 3182 - 3187
129245-23-4
→
反应条件
70-51-9
去铁胺
反应条件
1: 96 percent / pyridine 2: 95 percent / diphenyl phosphorazidate, triethylamine / dimethylformamide / 17 h / 0 - 20 °C 3: 100 percent / trifluoroacetic acid (TFA) / CH2Cl2 4: 91 percent / pyridine / 12 h 5: H2, HCl / 10percent Pd/C / methanol View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 11 p. 3182 - 3187
129245-22-3
→
反应条件
70-51-9
去铁胺
反应条件
1: 87 percent / trifluoroacetic acid (TFA) / CH2Cl2 / 0.75 h / 0 - 20 °C 2: 96 percent / pyridine 3: 95 percent / diphenyl phosphorazidate, triethylamine / dimethylformamide / 17 h / 0 - 20 °C 4: 100 percent / trifluoroacetic acid (TFA) / CH2Cl2 5: 91 percent / pyridine / 12 h 6: H2, HCl / 10percent Pd/C / methanol View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 11 p. 3182 - 3187
91905-05-4
(5-(羟基氨基)戊基)氨基甲酸苄酯
→
反应条件
70-51-9
去铁胺
反应条件
1: Py 2: acetic anhydride / 5 h / 95 - 100 °C 3: (i) H2, Pd-C, MeOH, (ii) /BRN= 898057/ 4: H2, aq. HCl / Pd-C / methanol View Scheme
参考文献
Helvetica Chimica Acta, , vol. 45, p. 631 - 637
92034-20-3
→
反应条件
70-51-9
去铁胺
反应条件
1: aq. NH4Cl, Zn / ethanol 2: Py 3: acetic anhydride / 5 h / 95 - 100 °C 4: (i) H2, Pd-C, MeOH, (ii) /BRN= 898057/ 5: H2, aq. HCl / Pd-C / methanol View Scheme
参考文献
Helvetica Chimica Acta, , vol. 45, p. 631 - 637
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