2-溴-N,2-二甲基-丙酰胺合成路线 (共 6 条)
反应条件
sodium hydrogencarbonate; sodium carbonate in dichloromethane
2 h;
参考文献
PIRAMED LIMITED
Patent: WO2006/46031 A1, 2006 ;
Location in patent: Page/Page column 52-53 ;
WO 2006/046031 A1
反应条件
in dichloromethane
-10 deg C to room temperature;
参考文献
Guziec, Frank S.; Torres, Felix F.
Journal of Organic Chemistry, 1993 , vol. 58, # 6 p. 1604 - 1606
参考文献
Safir et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 4840,4842
反应条件
sodium hydride
1.5 h; Mechanism;
参考文献
Scrimin, Paolo; D'Angeli, Feruccio; Veronese, Augusto C.; Baioni, Valentino
Tetrahedron Letters, 1983 , vol. 24, # 41 p. 4473 - 4476
参考文献
Scrimin, Paolo; D'Angeli, Ferruccio; Baioni, Valentino; Cavicchioni, Giorgio
Journal of Chemical Research, Miniprint, 1983 , # 10 p. 2237 - 2246
反应条件
water; silver(l) oxide in acetonitrile
3 h; Ambient temperature;
参考文献
Cavicchioni
Synthetic Communications, 1994 , vol. 24, # 16 p. 2223 - 2227