6-甲酰基-2-吡啶甲酸甲酯合成路线 （共 16 条）
反应条件
manganese(IV) oxide in dichloromethane T=25°C; 96 h;
参考文献
DeGoey, David A.; Flentge, Charles A.; Flosi, William J.; Grampovnik, David J.; Kempf, Dale J.; Klein, Larry L.
Patent: US2005/131017 A1, 2005 ;
Location in patent: Page/Page column 106 ;
反应条件
Dess-Martin periodane in dichloromethane 16 h;
参考文献
Wyeth
Patent: US2006/19965 A1, 2006 ;
Location in patent: Page/Page column 25-26 ;
US 20060019965 A1
反应条件
diisobutylaluminium hydride in dichloromethane T=-78°C; 3 h;
参考文献
Masiero, Stefano; Fini, Federico; Gottarelli, Giovanni; Spada, Gian Piero
Journal of Chemical Research, Miniprint, 1998 , # 10 p. 2736 - 2753
反应条件
1: 100 percent / SOCl2 / 3 h / Heating 2: 85 percent / NaBH4 / methanol / 4 h / 20 °C 3: 74 percent / MnO2 / acetone View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 4 p. 609 - 612
反应条件
selenium(IV) oxide; acetic acid
参考文献
Chemische Berichte, , vol. 86, p. 584,587
参考文献
Chemische Berichte, , vol. 86, p. 584,587
反应条件
methanol; aluminum oxide; palladium/alumina
参考文献
Mathes et al.
Chemische Berichte, 1953 , vol. 86, p. 584,587
反应条件
1: 80 percent / p-toluene sulfonic acid / toluene / 4 h / Heating 2: 1.) Na, CH3OH / benzene / 1.) 1 h, reflux, 2.) 16 h, r.t. 3: 3.5 percent HCl / 1 h / Heating View Scheme
参考文献
Budzikiewicz, H.; Hildebrand, U.; Ockels, W.; Reiche, M.; Taraz, K.
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 4 p. 516 - 520
参考文献
Mathes et al.
Chemische Berichte, 1953 , vol. 86, p. 584,587
反应条件
1: 80 percent / p-toluene sulfonic acid / toluene / 4 h / Heating 2: 1.) Na, CH3OH / benzene / 1.) 1 h, reflux, 2.) 16 h, r.t. 3: 3.5 percent HCl / 1 h / Heating 4: 30percent H2O2 / H2O View Scheme
参考文献
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, , vol. 38, # 4 p. 516 - 520
