1,4-双 (甲基磺酰基)苯合成路线 （共 7 条）
反应条件
1: MeSNa / 1.) HMPA, 100 deg C, 3 h; 2.) room temp. 2: Na / hexamethylphosphoric acid triamide / 100 °C View Scheme
参考文献
Testaferri, L.; Tiecco, M.; Tingoli, M.; Chianelli, D.; Montanucci, M.
Tetrahedron, 1982 , vol. 38, # 24 p. 3687 - 3692
反应条件
1: MeSNa / 1.) HMPA, 100 deg C, 3 h; 2.) room temp.
2: Na / hexamethylphosphoric acid triamide / 100 °C
3: Na / hexamethylphosphoric acid triamide / 100 °C
4: Na / hexamethylphosphoric acid triamide / 100 °C
View Scheme
参考文献
Testaferri, L.; Tiecco, M.; Tingoli, M.; Chianelli, D.; Montanucci, M.
Tetrahedron, 1982 , vol. 38, # 24 p. 3687 - 3692
反应条件
1: MeSNa / 1.) HMPA, 100 deg C, 3 h; 2.) room temp.
2: Na / hexamethylphosphoric acid triamide / 100 °C
3: Na / hexamethylphosphoric acid triamide / 100 °C
4: Na / hexamethylphosphoric acid triamide / 100 °C
View Scheme
参考文献
Testaferri, L.; Tiecco, M.; Tingoli, M.; Chianelli, D.; Montanucci, M.
Tetrahedron, 1982 , vol. 38, # 24 p. 3687 - 3692
反应条件
m-CBPA in dichloromethane
T=-20°C; 12 h;
参考文献
Kobayashi, Kenji; Koyama, Emiko; Namatame, Kazuhiko; Kitaura, Toyokazu; Kono, Chihiro; Goto, Mariko; Obinata, Takanobu; Furukawa, Naomichi
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3190 - 3195
反应条件
N(Et)4ClO4 in tetrahydrofuran; methanol
(electrolysis);
参考文献
Mancheno, Olga Garcia; Bolm, Carsten
Chemistry - A European Journal, 2007 , vol. 13, # 23 p. 6674 - 6681
反应条件
1: MeSNa / 1.) HMPA, 100 deg C, 3 h; 2.) room temp.
2: Na / hexamethylphosphoric acid triamide / 100 °C
3: Na / hexamethylphosphoric acid triamide / 100 °C
View Scheme
参考文献
Testaferri, L.; Tiecco, M.; Tingoli, M.; Chianelli, D.; Montanucci, M.
Tetrahedron, 1982 , vol. 38, # 24 p. 3687 - 3692
反应条件
1: nitric acid
2: concentrated hydriodic acid
3: glacial acetic acid; chlorine
View Scheme
参考文献
Zincke; Frohneberg
Chemische Berichte, 1909 , vol. 42, p. 2722 Anm.
Chemische Berichte, 1910 , vol. 43, p. 840
