2-(4-甲基苯基)乙醇合成路线 （共 73 条）
反应条件
[2,2']bipyridinyl; formic acid; [CpRu(η6-naphthalene)][PF6]; water in tetrahydrofuran T=55°C; 48 h;
参考文献
Li, Le; Herzon, Seth B.
Nature Chemistry, 2014 , vol. 6, # 1 p. 22 - 27
反应条件
sodium hydroxide in ethanol; water 3 h; Heating / reflux;
参考文献
CHATTOPADHYAYA, Jyoti
Patent: WO2007/64291 A1, 2007 ;
Location in patent: Page/Page column 17 ;
反应条件
methanol; Na-SG in tetrahydrofuran T=0 - 25°C; Bouveault-Blanc reduction; Inert atmosphere;
参考文献
Bodnar, Brian S.; Vogt, Paul F.
Journal of Organic Chemistry, 2009 , vol. 74, # 6 p. 2598 - 2600
反应条件
1: With [CpFe(CO)2(PCy3)][BF4]; phenyl silane T=100°C; 24 h; IrradiationNeat (no solvent)Inert atmosphere; 2: With hydrogenchloride; water in tetrahydrofuran T=20°C; 1 h;
参考文献
Bezier, David; Venkanna, Gopaladasu T.; Castro, Luis C. Misal; Zheng, Jianxia; Roisnel, Thierry; Sortais, Jean-Baptiste; Darcel, Christophe
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 10 p. 1879 - 1884
反应条件
aluminum oxide; sodium tetrahydroborate; palladium dichloride in hexane; water T=30°C; 1 h;
参考文献
Yakabe, Shigetaka
Synthetic Communications, 2010 , vol. 40, # 9 p. 1339 - 1344
反应条件
1: With benzo[1,3,2]dioxaborole; rhodium complex 2 in toluene T=20°C; Addition; Hydroboration; 2 h; 2: With sodium hydroxide; water; dihydrogen peroxide in toluene T=20°C; Oxidation; 2 h; Title compound not separated from byproducts;
参考文献
Chemistry - A European Journal, , vol. 5, # 4 p. 1320 - 1330
反应条件
(CO)3Fe(COD); phenyl silane in tetrahydrofuran T=20°C; 24 h; Inert atmosphereUV-irradiation; chemoselective reaction;
参考文献
Misal Castro, Luis C.; Li, Haoquan; Sortais, Jean-Baptiste; Darcel, Christophe
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 85 p. 10514 - 10516,3
反应条件
4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=0°C; Wittig rearrangement; 1 h;
参考文献
Gomez, Cecilia; Macia, Beatriz; Lillo, Victor J.; Yus, Miguel
Tetrahedron, 2006 , vol. 62, # 42 p. 9832 - 9839
反应条件
methanol; Na-SG in tetrahydrofuran T=0 - 25°C; Bouveault-Blanc reduction; Inert atmosphere;
参考文献
Bodnar, Brian S.; Vogt, Paul F.
Journal of Organic Chemistry, 2009 , vol. 74, # 6 p. 2598 - 2600
反应条件
triethylamine in 1,4-dioxane
