N-(4-呋喃-2-苯基)-乙酰胺合成路线 （共 7 条）
反应条件
palladium diacetate; sodium carbonate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in ethanol
T=85°C; Suzuki-Miyaura coupling; 36 h; Inert atmosphere;
参考文献
Molander, Gary A.; Canturk, Belgin; Kennedy, Lauren E.
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 973 - 980
反应条件
dichloro bis(acetonitrile) palladium(II) in acetonitrile
参考文献
Hashmi, A. Stephen K.; Choi, Ji-Hyun; Bats, Jan W.
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 1999 , vol. 341, # 4 p. 342 - 357
反应条件
1: 58 percent / diethyl ether / 0.5 h / 0 °C
2: Dess-Martin periodinane / CH2Cl2 / 0.33 h
3: silica gel
4: 3 percent / PdCl2(MeCN)2 / acetonitrile
View Scheme
参考文献
Hashmi, A. Stephen K.; Choi, Ji-Hyun; Bats, Jan W.
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 1999 , vol. 341, # 4 p. 342 - 357
反应条件
1: Dess-Martin periodinane / CH2Cl2 / 0.33 h
2: silica gel
3: 3 percent / PdCl2(MeCN)2 / acetonitrile
View Scheme
参考文献
Hashmi, A. Stephen K.; Choi, Ji-Hyun; Bats, Jan W.
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 1999 , vol. 341, # 4 p. 342 - 357
反应条件
1: Raney nickel, 80percent hydrazin hydrate / ethanol / 0.5 h / Heating
2: pyridine / 12 h / Ambient temperature
View Scheme
参考文献
Janda, Miroslav; Srogl, Jan; Dvorakova, Hana; Dvorak, Dalimil; Stibor, Ivan
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 4 p. 906 - 916
反应条件
1: 14.3 percent / isopentyl nitrite / neat (no solvent) / 24 h / 30 °C
2: Raney nickel, 80percent hydrazin hydrate / ethanol / 0.5 h / Heating
3: pyridine / 12 h / Ambient temperature
View Scheme
参考文献
Janda, Miroslav; Srogl, Jan; Dvorakova, Hana; Dvorak, Dalimil; Stibor, Ivan
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 4 p. 906 - 916
反应条件
pyridine
12 h; Ambient temperature;
参考文献
Janda, Miroslav; Srogl, Jan; Dvorakova, Hana; Dvorak, Dalimil; Stibor, Ivan
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 4 p. 906 - 916
