4-碘-N,N-二甲基苯胺合成路线 （共 56 条）
反应条件
tetraethylammonium p-toluenesulfonate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide Ambient temperatureelectrolysis;
参考文献
Tetrahedron Letters, , vol. 26, # 13 p. 1655 - 1658
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetraethylammonium p-toluenesulfonate; triphenylphosphine in N,N-dimethyl-formamide Ambient temperatureelectroreduction;
参考文献
Chemistry--A European Journal, , vol. 2, # 8 p. 957 - 966
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in dimethyl sulfoxide 6 h;
参考文献
Ishiyama, Tatsuo; Ishida, Kousaku; Miyaura, Norio
Tetrahedron, 2001 , vol. 57, # 49 p. 9813 - 9816
反应条件
1: 4-iodo-N,N-dimethylaniline With tBu4ZnLi2 in tetrahydrofuran T=-78 - 0°C; Inert atmosphere; 2: allyl bromide in tetrahydrofuran T=20°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Furayama, Taniyuki; Yonehara, Mitsuhiro; Arimoto, Sho; Kobayashi, Minoru; Matsumoto, Yotaro; Uchiyama, Masanobu
Chemistry - A European Journal, 2008 , vol. 14, # 33 p. 10348 - 10356
反应条件
in acetonitrile UV-irradiation; Quantum yield; Further Variations:Solvents;
参考文献
Freccero, Mauro; Fagnoni, Maurizio; Albini, Angelo
Journal of the American Chemical Society, 2003 , vol. 125, # 43 p. 13182 - 13190
反应条件
N-ethyl-N,N-diisopropylamine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; tris-(o-tolyl)phosphine in 1-methyl-pyrrolidin-2-one T=20°C; Reduction; silylation; 1 h;
参考文献
Murata, Miki; Suzuki, Katsuhiro; Watanabe, Shinji; Masuda, Yuzuru
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8569 - 8571
反应条件
hydrogen; potassium carbonate in 1,4-dioxane T=120 - 140°C; P=30003 Torr; 20 h; Autoclave;
参考文献
Hamasaki, Akiyuki; Yasutake, Yutaro; Norio, Takafumi; Ishida, Tamao; Akita, Tomoki; Ohashi, Hironori; Yokoyama, Takushi; Honma, Tetsuo; Tokunaga, Makoto
Applied Catalysis A: General, 2014 , vol. 469, p. 146 - 152
反应条件
potassium carbonate; bis-triphenylphosphine-palladium(II) chloride in various solvent(s) T=80°C; 5 h;
参考文献
Ishiyama, Tatsuo; Kizaki, Hiroe; Hayashi, Takahiro; Suzuki, Akira; Miyaura, Norio
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4726 - 4731
反应条件
potassium phosphate; Pd0(tris(tert-butyl)phosphine)2 in 1-methyl-pyrrolidin-2-one T=20°C; 5 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 23 p. 9607 - 9609
反应条件
N-ethyl-N,N-diisopropylamine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; tris-(o-tolyl)phosphine in 1-methyl-pyrrolidin-2-one T=20°C; Reduction; silylation; 1 h;
参考文献
Murata, Miki; Suzuki, Katsuhiro; Watanabe, Shinji; Masuda, Yuzuru
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8569 - 8571
