4-氯-N,N-二甲基苯胺合成路线 (共 152 条)
反应条件
Me2SCl2 in dichloromethane T=-25°C; 4 h;
参考文献
Synthesis, , # 10 p. 868 - 870
反应条件
Zr(BH4)2Cl2(dabco)2; zirconium tetrachloride in methanol; water T=20°C; 0.1 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 76, # 1 p. 143 - 151
反应条件
cis-[Ru(dimethyl sulfoxide)4Cl2]; phenyl silane; di-(1-adamantyl)-n-butylphosphine in toluene T=100°C; P=22502.3 Torr; AutoclaveInert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 36 p. 9568 - 9571
Angew. Chem., , vol. 125, # 36 p. 9747 - 9750,4
反应条件
ruthenium trichloride; tri-n-butyl phosphite in 1,4-dioxane T=180°C; 15 h;
参考文献
Chemistry Letters, , p. 449 - 452
反应条件
1: With copper dichloride in acetonitrile T=24 - 26°C; 10 h; 2: With potassium carbonate T=24 - 26°C; 0.166667 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 26 p. 9849 - 9852
参考文献
Journal of the American Chemical Society, , vol. 68, p. 895
参考文献
Journal of Organic Chemistry, , vol. 66, # 3 p. 677 - 680
反应条件
methanol; hydrogen T=99.84°C; P=9750.98 Torr; 1 h; Autoclave; Catalytic behavior; Reagent/catalystTimePressureSolvent;
参考文献
Catalysis Communications, , vol. 41, p. 115 - 118
反应条件
Ru(Triphos)(TMM); hydrogen; bis-(trifluoromethylsulphonyl)amine in tetrahydrofuran T=150°C; P=60006 Torr; 10 h; AutoclaveInert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 36 p. 9554 - 9557
Angew. Chem., , vol. 125, # 36 p. 9733 - 9736
反应条件
sodium hydroxide T=140°C;
参考文献
Journal of the Chemical Society, , p. 614,615