2',3',5'-三乙酰鸟苷合成路线 （共 42 条）
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in acetonitrile T=0 - 20°C; 4 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 51 p. 18133 - 18142
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=20°C; 1 h;
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 20, # 1-2 p. 59 - 75
反应条件
trimethylsilyl iodide 1 h; Ambient temperature;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 32, p. 2048 - 2051
参考文献
Journal of Biological Chemistry, , vol. 97, p. 491,493
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, , vol. 120, p. 126,127
反应条件
1: 92 percent / Bu4NIO4; RuCl3 / CH2Cl2; acetonitrile; H2O / 0.5 h / 20 °C 2: 96 percent / DBU / acetonitrile / 1 h / 20 °C View Scheme
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 20, # 1-2 p. 59 - 75
反应条件
1.1: hydrazine hydrate; AcOH; pyridine / 0.5 h / 20 °C 1.2: 96 percent / pyridine / 1 h / 20 °C 2.1: 92 percent / Bu4NIO4; RuCl3 / CH2Cl2; acetonitrile; H2O / 0.5 h / 20 °C 3.1: 96 percent / DBU / acetonitrile / 1 h / 20 °C View Scheme
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 20, # 1-2 p. 59 - 75
反应条件
1: sodium azide / N,N-dimethyl-formamide / 2 h / 50 °C 2: oxygen / acetonitrile; water / 0.33 h / 20 °C / |UV-irradiation View Scheme
参考文献
Photochemical and Photobiological Sciences, , vol. 13, # 3 p. 563 - 573
参考文献
Chemische Berichte, , vol. 80, p. 401,404
反应条件
acetic acid in ethanol; water 6 h; Heating;
参考文献
Tetrahedron Letters, , vol. 36, # 43 p. 7881 - 7884
反应条件
1: POCl3, N,N-diethylaniline / 1 h / 70 °C 2: 84 percent / (C2H5)3N / tetrahydrofuran / 17 h / 25 °C / Irradiation 3: 96 percent / NH3(g) / ethanol / 23 h / 25 °C View Scheme
参考文献
Nair; Young; DeSilvia Jr.
Journal of Organic Chemistry, 1987 , vol. 52, # 7 p. 1344 - 1347
