1-甲基-5-(3-硝基苯基)-1H-四唑合成路线 (共 3 条)
反应条件
sodium azide; trifluoromethanesulfonic acid anhydride in acetonitrile
T=0°C; 3.5 h;
参考文献
Batt, Douglas G.
Patent: US2004/67935 A1, 2004 ;
Location in patent: Page/Page column 28 ;
US 20040067935 A1
反应条件
sodium azide; tetrachlorosilane in acetonitrile
24 h; Ambient temperature;
参考文献
El-Ahl, Abdel-Aziz S.; Elmorsy, Saad S.; Soliman, Hanan; Amer, Fathy A.
Tetrahedron Letters, 1995 , vol. 36, # 40 p. 7337 - 7340
反应条件
in acetonitrile
T=25°C; other temperature. Other object of study : energy data; KineticsRate constantProduct distribution;
参考文献
Ostrovskii, V. A.; Shirobokov, I. Yu.; Koldobskii, G. I.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 131 - 135
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 146 - 151