5-氯-3,4-二氢-1H-2-萘酮合成路线 （共 7 条）
反应条件
sodium hydrogencarbonate; trifluoroacetic acid in dichloromethane
参考文献
Chen, Li; Cheung, Adrian Wai-Hing; Chu, Xin-Jie; Danho, Waleed; Swistok, Joseph; Wang, Yao; Yagaloff, Keith Alan
Patent: US2002/143141 A1, 2002 ;
US 20020143141 A1
反应条件
titanium tetrachloride in dichloromethane T=-78 - 20°C; 5 h;
参考文献
Hon, Yung-Son; Devulapally, Rammohan
Tetrahedron Letters, 2009 , vol. 50, # 23 p. 2831 - 2834
反应条件
aluminium trichloride in dichloromethane 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
European Journal of Medicinal Chemistry, , vol. 28, # 9 p. 693 - 701
反应条件
1: thionyl chloride / 1,2-dichloro-ethane / 4 h / Heating 2: 1.74 g / AlCl3 / CH2Cl2 / -5 - 5 °C View Scheme
参考文献
Synthetic Communications, , vol. 33, # 13 p. 2215 - 2227
反应条件
rhodium (II) acetate in dichloromethane Buchner reaction; Heating;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 1 p. 133 - 137
反应条件
1: SOCl2 / toluene / Heating 2: diethyl ether / 0 - 20 °C 3: Rh(OAc)2 / CH2Cl2 / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 1 p. 133 - 137
反应条件
1: diethyl ether / 0 - 20 °C 2: Rh(OAc)2 / CH2Cl2 / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 1 p. 133 - 137
