iodine in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide Kinetics; at -78°C in THF/hexamethylphosphoramide (3:1), for 30 h; analysis by GLC;
参考文献
Journal of the American Chemical Society, , vol. 111, p. 1804 - 1814
iodine in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide Kinetics; at -78°C in THF/hexamethylphosphoramide (3:1), for 30 h; analysis by GLC;
参考文献
Journal of the American Chemical Society, , vol. 111, p. 1804 - 1814
in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide at -78°C in THF/hexamethylphosphoramide (3:1), after 1 h at -60°C the reaction is worked up;
参考文献
Journal of the American Chemical Society, , vol. 111, p. 1804 - 1814
iodine in toluene; benzene at 22-24°C, under argon, succesive addn. of iodine, stirred overnight; diluted with ether, filtered through silica gel, solvent removed in vac.; 79percent of toluene-complex in equil. mixt. (determined by HPLC);
参考文献
Journal of the American Chemical Society, , vol. 106, p. 1487 - 1489
