1-(4-羟基-1-苯并呋喃-5-基)乙酮合成路线 (共 15 条)
反应条件
1: alkali View Scheme
参考文献
Sinha, B.; Bhat, V. S.; Joshi, V. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 519 - 520
反应条件
pyridine T=100°C; 0.166667 h;
参考文献
Dixit, Manish; Tripathi, Brajendra K.; Tamrakar, Akhilesh K.; Srivastava, Arvind K.; Kumar, Brijesh; Goel, Atul
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 2 p. 727 - 734
反应条件
1: 70 mg / KOH / ethanol / 75 h / 20 °C 2: 0.51 g / 30 percent aq. H2O2; aq. NaOH; pyridine / 60 - 70 °C 3: 0.68 g / K2CO3 / acetone / 2 h / Heating View Scheme
参考文献
Hossain, M. Amzad; Das; Salehuddin
Pakistan Journal of Scientific and Industrial Research, 2003 , vol. 46, # 1 p. 31 - 32
反应条件
potassium hydroxide in ethanol; water T=20°C; Claisen Schmidt condensation; 24 h;
参考文献
Rao, R. Ranga; Tiwari, Ashok K.; Reddy, P. Prabhakar; Babu, K. Suresh; Suresh; Ali, A. Zehra; Madhusudana; Agawane, Sachin B.; Badrinarayan, Preethi; Sastry, G. Narahari; Rao, J. Madhusudana
Medicinal Chemistry Research, 2012 , vol. 21, # 6 p. 760 - 774
反应条件
1: 90 percent / K2CO3 / dimethylformamide / 160 °C
2: 38 percent / Amberlyst 15 / toluene / 120 °C
View Scheme
参考文献
Dixit, Manish; Sharon, Ashoke; Maulik, Prakas R.; Goel, Atul
Synlett, 2006 , # 10 p. 1497 - 1502
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane
3 h; Heating;
参考文献
Lee, Yong Rok; Morehead, Andrew T.
Tetrahedron, 1995 , vol. 51, # 17 p. 4909 - 4922
反应条件
potassium hydroxide in ethanol
5 h; Heating;
参考文献
Talapatra, Sunil K.; Mallik, Asok K.; Talapatra, Bani
Phytochemistry (Elsevier), 1982 , vol. 21, # 3 p. 761 - 766
反应条件
1: With osmium(VIII) oxide; potassium meta-periodate in water; ethyl acetate
2: With phosphoric acid
0.333333 h; Heating;
参考文献
Hossain, M. Amzad; Das; Salehuddin
Pakistan Journal of Scientific and Industrial Research, 2003 , vol. 46, # 1 p. 31 - 32
反应条件
1.1: 1.3 g / 2 h / 210 - 215 °C
2.1: OsO4; KIO4 / ethyl acetate; H2O
2.2: 230 mg / H3PO4 / 0.33 h / Heating
View Scheme
参考文献
Hossain, M. Amzad; Das; Salehuddin
Pakistan Journal of Scientific and Industrial Research, 2003 , vol. 46, # 1 p. 31 - 32
反应条件
1: K2CO3; acetone
2: aqueous alkaline solution
3: sodium acetate; acetic acid anhydride
View Scheme
参考文献
Rao et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 685