acetonitrile in diethylene glycol
(Ar); to soln. of Mo-acetonitrile complex (from Mo(CO)6 and MeCN) was added fulvenderiv., mixt. was heated at 60-70°C for 2 and left to stand overnight at room temp.; formed crystals were filtered off, washed with hexane and dried in vac.(1 mmHg, 50-60°C, 6 h); from mother liquor was obtained 2nd cropby pptn. with hexane and drying as above; elem. anal.;
参考文献
Setkina, V. N.; Strunin, B. N.; Kursanov, D. N.
Journal of Organometallic Chemistry, 1980 , vol. 186, # 3 p. 325 - 330
