1-(4-氯苯基)-1-苯基-2,2-二氯乙烷合成路线 （共 7 条）
反应条件
hydrogen; triethylamine; palladium on activated charcoal in methanol
T=20°C; 0.0833333 h;
参考文献
Monguchi, Yasunari; Kume, Akira; Sajiki, Hironao
Tetrahedron, 2006 , vol. 62, # 35 p. 8384 - 8392
反应条件
1: 12 percent / H2; Et3N / Pd/C / methanol / 0.5 h / 20 °C
2: 21 percent / H2; Et3N / Pd/C / methanol / 0.08 h / 20 °C
View Scheme
参考文献
Monguchi, Yasunari; Kume, Akira; Sajiki, Hironao
Tetrahedron, 2006 , vol. 62, # 35 p. 8384 - 8392
反应条件
hydrogen; palladium on activated charcoal
T=20°C; 24 h;
参考文献
Monguchi, Yasunari; Kume, Akira; Sajiki, Hironao
Tetrahedron, 2006 , vol. 62, # 35 p. 8384 - 8392
反应条件
1: nBuLi
2: SO3/H2SO4
View Scheme
参考文献
Bal'on,Ya.G.; Shul'man,M.D.
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 9 p. 1973 - 1979,1926 - 1931
反应条件
sulfuric acid; sulfur trioxide
参考文献
Bal'on,Ya.G.; Shul'man,M.D.
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 9 p. 1973 - 1979,1926 - 1931
反应条件
palladium/alumina
T=220°C; P=2.3 Torr; in pulse microreactor, injected from p-xylene solution; Product distribution;
参考文献
Weiss, A. H.; LaPierre, R. B.
Acta Chimica Academiae Scientiarum Hungaricae, 1980 , vol. 103, # 1 p. 111 - 122
反应条件
T=225°C; P=2.3 Torr; in pulse microreactor, injected from p-xylene solution; α-Al2O3 catalyst with/without Pd additive; Product distribution;
参考文献
Weiss, A. H.; LaPierre, R. B.
Acta Chimica Academiae Scientiarum Hungaricae, 1980 , vol. 103, # 1 p. 111 - 122
