1-O-苯甲酰基-1,3-丙烷二醇合成路线 （共 25 条）
反应条件
1H-imidazole; iodine; triphenylphosphine in benzene 0.666667 h; Heating;
参考文献
Thompson, Andrew M.; Delaney, Amy M.; Hamby, James M.; Schroeder, Mel C.; Spoon, Teresa A.; Crean, Sheila M.; Showalter, H. D. Hollis; Denny, William A.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 14 p. 4628 - 4653
反应条件
aluminum oxide; Oxonereg;; water in chloroform
T=50°C; 3 h;
参考文献
Curini, Massimo; Epifano, Francesco; Marcotullio, Maria Carla; Rosati, Ornelio
Synlett, 1999 , # 6 p. 777 - 779
反应条件
di-methyltin dichloride; potassium carbonate in tetrahydrofuran
12 h; Ambient temperature;
参考文献
Iwasaki, Fumiaki; Maki, Toshihide; Onomura, Osamu; Nakashima, Waka; Matsumura, Yoshihiro
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 996 - 1002
反应条件
hydrogen; palladium on activated charcoal in ethanol
P=760 Torr; Ambient temperature;
参考文献
Mukaiyama, Teruaki; Ohshima, Masahiro; Murakami, Masahiro
Chemistry Letters, 1984 , p. 265 - 266
反应条件
pyridinium hydrobromide perbromide in water
T=20°C; 45 h;
参考文献
Sayama, Shinsei; Onami, Tetsuo
Synlett, 2004 , # 15 p. 2739 - 2745
反应条件
pyridinium bromide perbromide in methanol
T=-20°C; 1.5 h;
参考文献
Martinez-Solorio, Dionicio; Jennings, Michael P.
Tetrahedron Letters, 2008 , vol. 49, # 35 p. 5175 - 5178
反应条件
aluminium trichloride; N,N-dimethyl-aniline in dichloromethane
1 h; Ambient temperature;
参考文献
Akiyama, Takahiko; Hirofuji, Hajimu; Ozaki, Shoichiro
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 7 p. 1932 - 1938
反应条件
tert.-butylhydroperoxide; [bis(acetoxy)iodo]benzene in acetic acid n-butyl ester
T=0 - 25°C; 12 h;
参考文献
Zhao, Yi; Ang, Jascelyn Qian Lin; Ng, Angela Wan Ting; Yeung, Ying-Yeung
RSC Advances, 2013 , vol. 3, # 43 p. 19765 - 19768
反应条件
triethylamine in acetonitrile
T=0°C; 3 h;
参考文献
Holy, Antonin; Kohoutova, Jitka; Merta, Ales; Votruba, Ivan
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 2 p. 459 - 477
反应条件
1: in dichloromethane
T=20°C; 3 h; Inert atmosphere;
2: With water; sodium hydrogencarbonate in dichloromethane
Saturated solution; chemoselective reaction;
参考文献
Wakita, Natsumi; Hara, Shoji
Tetrahedron, 2010 , vol. 66, # 40 p. 7939 - 7945
