2-氯双环[2.2.1]庚-5-烯-2-甲腈合成路线 (共 4 条)
反应条件
1: With lithium diisopropyl amide in tetrahydrofuran T=-78 - 20°C; 2: With 2-chloro-2-fluoro-2-phenylacetonitrile in tetrahydrofuran T=-78°C; 0.0833333 h;
参考文献
Organic Letters, , vol. 12, # 12 p. 2810 - 2813
反应条件
in benzene T=40°C; 1344 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Canadian Journal of Chemistry, , vol. 62, p. 1751 - 1766
反应条件
hydroquinone T=150°C; Diels-Alder reaction; 1 h; Microwave irradiation; optical yield given as percent de;
参考文献
Synthesis, , # 24 art. no. Z80411SS, p. 4077 - 4083
反应条件
potassium hydroxide in water; dimethyl sulfoxide 48 h; Ambient temperature;
参考文献
Drian, Claude Le; Greene, Andrew E.
Journal of the American Chemical Society, 1982 , vol. 104, # 20 p. 5473 - 5483