5-溴异吲哚-1,3-二酮合成路线 （共 29 条）
反应条件
formamide T=200°C; 2 h;
参考文献
US2010/204214 A1, ;
Page/Page column 109 ;
反应条件
sulfuric acid; formamide in diethylene glycol dimethyl ether T=130 - 140°C; 7 h;
参考文献
US2006/142553 A1, ;
Page/Page column 13-14 ;
反应条件
sulfuric acid; sodium nitrite anschliessend mit Kaliumbromid und Kupfer-Pulver;
参考文献
Journal of the Chemical Society, , p. 2466,2469
反应条件
ammonium thiocyanate T=160°C; 0.166667 h;
参考文献
Helvetica Chimica Acta, , vol. 87, # 4 p. 825 - 844
反应条件
1: 65 percent / Br2 2: 84 percent / NH4SCN / 0.17 h / 160 °C View Scheme
参考文献
Helvetica Chimica Acta, , vol. 87, # 4 p. 825 - 844
反应条件
ammonia; oxygen T=359.84°C; 0.000519444 h; Inert atmosphere; Mechanism; TimeTemperatureConcentration;
参考文献
Russian Journal of General Chemistry, , vol. 80, # 8 p. 1672 - 1676
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 126, p. 69,72
反应条件
V–Sb–Bi–Zr/γ-Al2O3-oxide catalyst T=359.84°C; Kinetics; Solvent;
参考文献
Russian Journal of General Chemistry, , vol. 83, # 3 p. 492 - 495
Zh. Obshch. Khim., , vol. 83, # 3 p. 439 - 442,4
反应条件
ammonia; oxygen KineticsEquilibrium constantActivation energy; PressureTemperatureTime;
参考文献
Russian Journal of General Chemistry, , vol. 80, # 9 p. 1779 - 1785
反应条件
1: 5-bromo-1,3-dihydro-1,3-dioxo-2H-isoindole With sodium hydride in DMF (N,N-dimethyl-formamide) T=20°C; 0.25 h; 2: methyl iodide in DMF (N,N-dimethyl-formamide) T=20°C; 0.5 h;
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/73205 A1, 2005 ;
Location in patent: Page/Page column 35 ;
WO 2005/073205 A1
