1,2,3,6-四氢吡啶合成路线 (共 66 条)
反应条件
[{(η5-C5Me5)IrCl}2(μ-Cl)2]; triethylammonium formate; potassium iodide in dichloromethane T=40°C; 24 h; Sealed tube;
参考文献
Wu, Jianjun; Tang, Weijun; Pettman, Alan; Xiao, Jianliang
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 1 p. 35 - 40
反应条件
potassium tert-butylate T=60°C; P=0.001 Torr; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 44, # 14 p. 4447 - 4456
反应条件
1: NaBH4 / ethanol / 6 h / 20 °C 2: 93 percent / benzene / 1 h / Heating 3: NH2NH2*H2O; KOH / ethane-1,2-diol / 1.5 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 16 p. 4523 - 4526
参考文献
Doklady Chemistry, , vol. 391, # 4-6 p. 195 - 199
反应条件
potassium hydroxide; hydrazine hydrate in ethylene glycol 1.5 h; Heating;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 16 p. 4523 - 4526
反应条件
samarium diiodide in tetrahydrofuran; water 0.15 h; Ambient temperature;
参考文献
Heterocycles, , vol. 36, # 10 p. 2383 - 2396
反应条件
1: acetonitrile / 0.25 h / 85 °C / |Reflux 2: [{(η5-C5Me5)IrCl}2(μ-Cl)2]; potassium iodide; triethylammonium formate / dichloromethane / 24 h / 40 °C / |Sealed tube View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 1 p. 35 - 40
反应条件
sulfuric acid Electrolysis;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 24, p. 1029,1031, 1033
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 19, p. 502
反应条件
1: diethyl ether 2: aqueous hydrochloric acid View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 19, p. 502