1: in diethyl ether
T=0 - 23°C; 3 h; Inert atmosphere;
2: With tert-butylhypochlorite in tetrachloromethane
T=23°C; 1 h; Inert atmosphere;
参考文献
Powers, David C.; Lee, Eunsung; Ariafard, Alireza; Sanford, Melanie S.; Yates, Brian F.; Canty, Allan J.; Ritter, Tobias
Journal of the American Chemical Society, 2012 , vol. 134, # 29 p. 12002 - 12009
Moss, Robert A.; Wilk, Boguslawa; Krogh-Jespersen, Karsten; Blair, John T.; Westbrook, John D.
Journal of the American Chemical Society, 1989 , vol. 111, # 1 p. 250 - 258
1.1: potassium carbonate / N,N-dimethyl-formamide / 14 h / 23 °C
2.1: diethyl ether / 3 h / 0 - 23 °C / Inert atmosphere
2.2: 1 h / 23 °C / Inert atmosphere
View Scheme
参考文献
Powers, David C.; Lee, Eunsung; Ariafard, Alireza; Sanford, Melanie S.; Yates, Brian F.; Canty, Allan J.; Ritter, Tobias
Journal of the American Chemical Society, 2012 , vol. 134, # 29 p. 12002 - 12009
acetic acid; triphenylphosphine in dichloromethane
T=23°C; 0.0833333 h;
参考文献
Powers, David C.; Lee, Eunsung; Ariafard, Alireza; Sanford, Melanie S.; Yates, Brian F.; Canty, Allan J.; Ritter, Tobias
Journal of the American Chemical Society, 2012 , vol. 134, # 29 p. 12002 - 12009
