N-(2-羟基乙基)甲酰胺合成路线 (共 21 条)
反应条件
thionyl chloride 1 h; Ambient temperature;
参考文献
Smith, Forrest T.; Atigadda, Ram V.
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 7 p. 1813 - 1816
参考文献
Robinson Brothers Limited
Patent: US4673748 A1, 1987 ;
反应条件
thionyl chloride zuletzt in der Waerme;
参考文献
Levine, Mindy; Kenesky, Craig S.; Zheng, Shengping; Quinn, Jordan; Breslow, Ronald
Tetrahedron Letters, 2008 , vol. 49, # 40 p. 5746 - 5750
反应条件
triethylamine in dichloromethane 1 h; Heating;
参考文献
Fehlhammer, Wolf Peter; Bartel, Klaus; Weinberger, Bernd; Plaia, Ulrike
Chemische Berichte, 1985 , vol. 118, # 6 p. 2220 - 2234
反应条件
beim Erhitzen oder bei der Einwirkung von wasserabspaltenden Mitteln;
参考文献
Wenker
Journal of the American Chemical Society, 1935 , vol. 57, p. 1080
反应条件
indium
T=70°C; 2 h; neat (no solvent); chemoselective reaction;
参考文献
Kim, Joong-Gon; Jang, Doo Ok
Synlett, 2010 , # 8 art. no. U00810ST, p. 1231 - 1234
反应条件
1: ethanolamine With sodium ethanolate
T=20°C; 0.5 h;
2: formic acid ethyl ester in ethanol
1 h; Heating; Further stages.;
参考文献
Levine, Mindy; Kenesky, Craig S.; Zheng, Shengping; Quinn, Jordan; Breslow, Ronald
Tetrahedron Letters, 2008 , vol. 49, # 40 p. 5746 - 5750
反应条件
acetic anhydride; potassium carbonate; formamide
参考文献
Beckman, Eric J.; Chapman, Toby M.; Favero, Cedrick; Capelli, Christopher C.; Swift, Harold E.; Carroll, William Eamon
Patent: US2005/33089 A1, 2005 ;
反应条件
1,4-dioxo-1,2,3,4-tetrahydro-phthalazine
T=80 - 95°C; 40 h;
参考文献
Iwata, Masaaki; Kuzuhara, Hiroyoshi
Chemistry Letters, 1989 , p. 2029 - 2030
反应条件
benzoic acid methyl ester
T=200°C; 0.0833333 h; Microwave irradiation;
参考文献
Yang, Dongsik; Jeon, Heung Bae
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 5 p. 1424 - 1426