反应条件
1: LAH
2: 90 percent / HCl / 1) 0 deg C, 4h, 2) r.t., 24h
3: 97 percent / m-chloroperbenzoic acid, Na-acetate / CHCl3 / 3 h
4: 1) butyl lithium, diisopropylamine / 1) ether, 1h, 2) 6h, reflux
5: 60 percent / pyridinium chlorochromate / CH2Cl2 / 2 h / Ambient temperature
6: 50 percent / tetrahydrofuran / 1) r.t., 6h, 2) 45 deg C, 1h
7: 92 percent / PTS / methanol / 4 h
View Scheme
参考文献
Vig, O. P.; Sharma, M. L.; Verma, N. K.; Malik, Neera
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 8 p. 692 - 694
