二(仲-丁基)汞(II)合成路线 （共 15 条）
反应条件
tetrabutylammomium bromide; oxygen in benzene 5 h; Ambient temperature; Yields of byproduct given;
参考文献
Doklady Chemistry, , vol. 257, p. 136 - 137
Dokl. Akad. Nauk SSSR Ser. Khim., , vol. 257, # 4 p. 896 - 897
反应条件
oxygen; tetrabutylammomium bromide in 1,2-dichloro-ethane; benzene other reaction conditions; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, # 8 p. 1386 - 1389
Zhurnal Organicheskoi Khimii, , vol. 18, # 8 p. 1584 - 1588
反应条件
diethyl ether; iodine
参考文献
Tafel
Chemische Berichte, 1906 , vol. 39, p. 3628
反应条件
T=500°C; P=3 - 5 Torr; Pyrolysis;
参考文献
Frey; Hepp
Journal of the American Chemical Society, 1933 , vol. 55, p. 3358
反应条件
T=500°C; P=3 - 5 Torr; Pyrolysis;
参考文献
Frey; Hepp
Journal of the American Chemical Society, 1933 , vol. 55, p. 3358
反应条件
in acetonitrile T=20°C; Yields of byproduct given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, # 6 p. 1231 - 1234
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1382 - 1386
反应条件
potassium bromide in nitromethane byproducts: Ph2CH2, Ph2CH(sec-Bu); Ar atmosphere and absence of light and moisture; addn. of AgBF4 in nitromethane to soln. of alkylmercury, portionwise addn. of Ph2CHCl in nitromethane (20°C, TLC monitoring), washing with soln. of KBr; TLC;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, # 6 p. 1231 - 1234
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1382 - 1386
反应条件
in acetonitrile
T=20°C; Yields of byproduct given;
参考文献
Uglova, E. V.; Petrovskii, K. B.; Fadeeva, S. S.; Mikhura, I. V.; Reutov, O. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 6 p. 1231 - 1234
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 6 p. 1382 - 1386
反应条件
potassium bromide in nitromethane
byproducts: Ph2CH2, Ph2CH(sec-Bu); Ar atmosphere and absence of light and moisture; addn. of AgBF4 in nitromethane to soln. of alkylmercury, portionwise addn. of Ph2CHCl in nitromethane (20°C, TLC monitoring), washing with soln. of KBr; TLC;
参考文献
Uglova, E. V.; Petrovskii, K. B.; Fadeeva, S. S.; Mikhura, I. V.; Reutov, O. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 6 p. 1231 - 1234
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 6 p. 1382 - 1386
反应条件
oxygen; tetrabutylammomium bromide in 1,2-dichloro-ethane; benzene
other reaction conditions; Product distribution;
参考文献
Uglova, E. V.; Makhaev, V. D.; Reutov, O. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 8 p. 1386 - 1389
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 8 p. 1584 - 1588
