4-(羟甲基)苯甲酸甲酯合成路线 (共 132 条)
反应条件
sodium tetrahydroborate in ethanol T=5°C; 0.5 h;
参考文献
Battilocchio, Claudio; Hawkins, Joel M.; Ley, Steven V.
Organic Letters, 2013 , vol. 15, # 9 p. 2278 - 2281
反应条件
zinc(II) tetrahydroborate; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; diethyl ether T=0°C; 0.25 h;
参考文献
Kotsuki, Hiyoshizo; Ushio, Yasuyuki; Yoshimura, Naka; Ochi, Masamitsu
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 7 p. 2684 - 2686
反应条件
Benzyltriethylammonium borohydride in dichloromethane Reduction; Heating;
参考文献
Narasimhan; Swarnalakshmi; Balakumar
Synthetic Communications, 2000 , vol. 30, # 5 p. 941 - 946
反应条件
[Ru(II)(η6-benzene)(μ-Cl)Cl]2; 2-((di-p-tolylphosphino)methyl)-1-methyl-1H-imidazole; potassium tert-butylate; hydrogen in tetrahydrofuran T=100°C; P=37503.8 Torr; 4.5 h;
参考文献
Chemistry - A European Journal, , vol. 18, # 29 p. 9011 - 9018
反应条件
zinc(II) tetrahydroborate in tetrahydrofuran; diethyl ether T=40°C; 48 h;
参考文献
Kotsuki, Hiyoshizo; Yoshimura, Naka; Ushio, Yasuyuki; Ohtsuka, Tatsuya; Ochi, Masamitsu
Chemistry Letters, 1986 , p. 1003 - 1004
反应条件
cerium(III) chloride in methanol T=20°C; detetrahydropyranylation; 2 h;
参考文献
Reddy; Neelakantan; Iyengar
Synthetic Communications, 2000 , vol. 30, # 22 p. 4107 - 4111
反应条件
hydrogenchloride 4 h; Heating;
参考文献
Marsh, Ian R.; Bradley, Mark
Tetrahedron, 1997 , vol. 53, # 51 p. 17317 - 17334
反应条件
potassium hydrogensulfate in methanol T=20°C; 2 h;
参考文献
Arumugam, Pandurangan; Karthikeyan, Ganesan; Perumal, Paramasivan T.
Chemistry Letters, 2004 , vol. 33, # 9 p. 1146 - 1147
反应条件
water; silica gel; sodium iodide in acetone T=20°C; 24 h; Irradiation;
参考文献
Itoh, Akichika; Kodama, Tomohiro; Inagaki, Shinji; Masaki, Yukio
Organic Letters, 2001 , vol. 3, # 17 p. 2653 - 2656
反应条件
C57H43IP2Pd; triethylamine T=130°C; P=3750.38 Torr; 24 h; Autoclave;
参考文献
Kaganovsky, Luba; Gelman, Dmitri; Rueck-Braun, Karola
Journal of Organometallic Chemistry, 2010 , vol. 695, # 2 p. 260 - 266