(1Z)-N-甲基-1-苯基乙烷亚胺合成路线 （共 5 条）
反应条件
1: sulfur / 170 - 180 °C / im Rohr 2: aqueous alcoholic hydrochloric acid / 30 - 40 °C / Electrolysis.an Bleikathoden View Scheme
参考文献
Kindler
Justus Liebigs Annalen der Chemie, 1923 , vol. 431, p. 213
Chem. Zentralbl., 1923 , vol. 94, # II p. 403
反应条件
sulfur dioxide; soda-lime; zirconium oxide T=450°C;
参考文献
Amato, Joseph S.; Karady, Sandor; Phillips, Brian T.; Weinstock, Leonard M.
Heterocycles, 1984 , vol. 22, # 9 p. 1947 - 1949
反应条件
sulfur
T=170 - 180°C; im Rohr;
参考文献
Kindler
Justus Liebigs Annalen der Chemie, 1923 , vol. 431, p. 213
Chem. Zentralbl., 1923 , vol. 94, # II p. 403
反应条件
triethylamine in Petroleum ether
T=0°C; 0.0833333 h;
参考文献
Ahlbrecht, Hubertus; Dueber, Ernst-Otto
Synthesis, 1980 , # 8 p. 630 - 631
反应条件
1: 80 percent / CH2Cl2 / 0 °C
2: 93 percent / ethanol
3: 75 percent / Bu3SnH, azobisisobutyronitrile (AIBN) / toluene / 14.5 h / Heating
View Scheme
参考文献
Sato, Tatsunori; Machigashira, Naomi; Ishibashi, Hiroyuki; Ikeda, Masazumi
Heterocycles, 1992 , vol. 33, # 1 p. 139 - 142
