顺-1,4-二苄氧基-2-丁烯合成路线 （共 11 条）
反应条件
CoCl2 in acetonitrile Ambient temperature; Yields of byproduct given;
参考文献
Iqbal; Srivastava
Tetrahedron, 1991 , vol. 47, # 18-19 p. 3155 - 3170
反应条件
CoCl2 in acetonitrile Ambient temperature; Yields of byproduct given;
参考文献
Iqbal; Srivastava
Tetrahedron, 1991 , vol. 47, # 18-19 p. 3155 - 3170
反应条件
CoCl2 in acetonitrile Ambient temperature; Yields of byproduct given;
参考文献
Tetrahedron, , vol. 47, # 18-19 p. 3155 - 3170
反应条件
sodium tetrahydroborate; ozone in methanol; dichloromethane
参考文献
Cloarec, Jean-Manuel; Charette, Andre B.
Organic Letters, 2004 , vol. 6, # 25 p. 4731 - 4734
反应条件
1: With ozone in methanol T=-60°C; 2: With triphenylphosphine in methanol; ethyl acetate T=-60 - 20°C;
参考文献
Aoki, Tsutomu; Konoike, Toshiro
Patent: US2003/195363 A1, 2003 ;
Location in patent: Page/Page column 12-13 ;
反应条件
CoCl2 in acetonitrile Ambient temperature; Yields of byproduct given;
参考文献
Tetrahedron, , vol. 47, # 18-19 p. 3155 - 3170
反应条件
CoCl2 in acetonitrile Ambient temperature; Yields of byproduct given;
参考文献
Tetrahedron, , vol. 47, # 18-19 p. 3155 - 3170
反应条件
1: With Grubb's 2nd generation catalyst in dichloromethane T=40°C; 2: With triethylamine in dichloromethane T=0 - 20°C; 1 h; optical yield given as percent dechemoselective reaction;
参考文献
Kanemoto, Mitsunori; Murata, Michio; Oishi, Tohru
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8810 - 8813
反应条件
1: O3; NaBH4 / methanol; CH2Cl2
2: I2; PPh3; imidazole / toluene
3: 86 percent / n-BuLi; diisopropylamine / tetrahydrofuran / -78 - -10 °C
4: LiAlH4 / diethyl ether
5: 97 percent / (COCl)2; DMSO; Et3N / CH2Cl2
6: 73 percent / HMDS; n-BuLi; I2 / tetrahydrofuran / 0.17 h / -78 °C
View Scheme
参考文献
Cloarec, Jean-Manuel; Charette, Andre B.
Organic Letters, 2004 , vol. 6, # 25 p. 4731 - 4734
反应条件
1: O3; NaBH4 / methanol; CH2Cl2
2: I2; PPh3; imidazole / toluene
3: 86 percent / n-BuLi; diisopropylamine / tetrahydrofuran / -78 - -10 °C
View Scheme
参考文献
Cloarec, Jean-Manuel; Charette, Andre B.
Organic Letters, 2004 , vol. 6, # 25 p. 4731 - 4734
