三丁基(2-甲基苯基)锡烷合成路线 （共 36 条）
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; cesium fluoride in 1,4-dioxane
T=60°C; 20 h;
参考文献
Littke, Adam F.; Schwarz, Lothar; Fu, Gregory C.
Journal of the American Chemical Society, 2002 , vol. 124, # 22 p. 6343 - 6348
反应条件
[PdCl2(AsPh3)2]; [AuCl(AsPh3)]; triphenyl-arsane; lithium chloride in acetonitrile
T=80°C; Stille Cross Coupling; 6 h; Inert atmosphere;
参考文献
Delpozo, Juan; Carrasco, Desiree; Perez-Temprano, Monica H.; Garcia-Melchor, Max; Alvarez, Rosana; Casares, Juan A.; Espinet, Pablo
Angewandte Chemie - International Edition, 2013 , vol. 52, # 8 p. 2189 - 2193
Angew. Chem., 2013 , vol. 125, # 8 p. 2245 - 2249
反应条件
palladium diacetate; copper diacetate; anhydrous lithium acetate in N,N-dimethyl-formamide
T=100°C; 24 h;
参考文献
Hirabayashi, Kazunori; Ando, Jun-Ichi; Nishihara, Yasushi; Mori, Atsunori; Hiyama, Tamejiro
Synlett, 1999 , # 1 p. 99 - 101
反应条件
tris(dibenzylideneacetone)dipalladium (0); c-{P[-N(Bn)-CH2-CH2-]2N[-CH2-CH2-N(iBu)]}; cesium fluoride in 1,4-dioxane
T=115°C; Stille cross-coupling; 48 h;
参考文献
Su, Weiping; Urgaonkar, Sameer; McLaughlin, Patrick A.; Verkade, John G.
Journal of the American Chemical Society, 2004 , vol. 126, # 50 p. 16433 - 16439
反应条件
tris(dibenzylideneacetone)dipalladium (0); c-{P[-N(Bn)-CH2-CH2-]2N[-CH2-CH2-N(iBu)]}; cesium fluoride in 1,4-dioxane
T=115°C; Stille cross-coupling; 40 h;
参考文献
Su, Weiping; Urgaonkar, Sameer; McLaughlin, Patrick A.; Verkade, John G.
Journal of the American Chemical Society, 2004 , vol. 126, # 50 p. 16433 - 16439
反应条件
tris(dibenzylideneacetone)dipalladium (0); c-{P[-N(Bn)-CH2-CH2-]2N[-CH2-CH2-N(iBu)]}; cesium fluoride in 1,4-dioxane
T=20°C; Stille cross-coupling; 48 h;
参考文献
Su, Weiping; Urgaonkar, Sameer; McLaughlin, Patrick A.; Verkade, John G.
Journal of the American Chemical Society, 2004 , vol. 126, # 50 p. 16433 - 16439
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2; phenol in toluene
24 h; Heating;
参考文献
Koike, Tooru; Takahashi, Masabumi; Arai, Nobumichi; Mori, Atsunori
Chemistry Letters, 2004 , vol. 33, # 10 art. no. CL-040955, p. 1364 - 1365
反应条件
tris(dibenzylideneacetone)dipalladium (0); c-{P[-N(Bn)-CH2-CH2-]2N[-CH2-CH2-N(iBu)]}; cesium fluoride in 1,4-dioxane
T=115°C; Stille cross-coupling; 48 h;
参考文献
Su, Weiping; Urgaonkar, Sameer; McLaughlin, Patrick A.; Verkade, John G.
Journal of the American Chemical Society, 2004 , vol. 126, # 50 p. 16433 - 16439
反应条件
Pd((CH3)2C6H3NC(CH3)CHC(CH3)NC6H3(CH3)2)(CH3)(P(CH2CH3)3); cesium fluoride in tetrahydrofuran
T=50°C; Stille Cross Coupling; 6 h;
参考文献
Lee, Dong-Hwan; Qian, Yingjie; Park, Ji-Hoon; Lee, Jong-Suk; Shim, Sang-Eun; Jin, Myung-Jong
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1729 - 1735
反应条件
cesium fluoride in ethanol; water
T=50°C; Stille coupling; 10 h; Inert atmosphere;
参考文献
Lee, Dong-Hwan; Jung, Ji-Young; Jin, Myung-Jong
Green Chemistry, 2010 , vol. 12, # 11 p. 2024 - 2029
