(苯并-18-冠-6)-4′-基胺合成路线 (共 6 条)
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Dykes, Graham M.; Smith, David K.
Tetrahedron, 2003 , vol. 59, # 22 p. 3999 - 4009
参考文献
Acta Chimica Academiae Scientiarum Hungaricae, , vol. 110, # 1 p. 25 - 28
反应条件
1: 50 percent / 65percent nitric acid / CHCl3 / 0.5 h / 20 - 24 °C 2: 75 percent / 60percent aq. KOH / dicyclohexyl-18-crown-6 / tetrahydrofuran / 5 h / Heating 3: 71 percent / hydrazine hydrate / Pd/C / ethanol / 0.75 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 1305 - 1307
Zhurnal Organicheskoi Khimii, , vol. 18, # 7 p. 1495 - 1498
反应条件
1: 75 percent / 60percent aq. KOH / dicyclohexyl-18-crown-6 / tetrahydrofuran / 5 h / Heating 2: 71 percent / hydrazine hydrate / Pd/C / ethanol / 0.75 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 1305 - 1307
Zhurnal Organicheskoi Khimii, , vol. 18, # 7 p. 1495 - 1498
反应条件
1: NaHCO3 / methanol / 0.5 h
2: 32 percent / HNO3 / CHCl3; acetic acid / Ambient temperature
View Scheme
参考文献
Yamashita; Nakamura; Takagi; ueno
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 6 p. 1550 - 1554
反应条件
in chlorobenzene
Heating;
参考文献
Agai, B.; Bitter, I.; Csongor, E.; Toeke, L.
Acta Chimica Academiae Scientiarum Hungaricae, 1982 , vol. 110, # 1 p. 25 - 28