1-(3,4-亚甲二氧基苯基)-1-丙醇合成路线 (共 12 条)
反应条件
1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C / |Inert atmosphere
1.2: 8 h / 20 °C / |Inert atmosphere
2.1: anhydrous iron chloride / dichloromethane / 0.8 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Fan, Xiaohui; Fu, Lin-An; Li, Na; Lv, Hao; Cui, Xiao-Meng; Qi, Yuan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 13 p. 2147 - 2153
反应条件
silica gel in 1,4-dioxane
0.05 h; microwave irradiation;
参考文献
Sharma, Anuj; Joshi, Bhupendra P.; Sinha, Arun K.
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 12 p. 2231 - 2235