3-羟基-4-甲氧基黄酮合成路线 （共 35 条）
反应条件
dihydrogen peroxide; sodium hydroxide in methanol; water T=20°C;
参考文献
Dias, Tatiana A.; Duarte, Cecilia L.; Lima, Cristovao F.; Proenca, M. Fernanda; Pereira-Wilson, Cristina
European Journal of Medicinal Chemistry, 2013 , vol. 65, p. 500 - 510
参考文献
Dhoubhadel, S. P.; Tuladhar, Sudersan M.; Tuladhar, Sarbajna M.; Wagley, Pradyumna P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 511 - 512
反应条件
sodium hydroxide; water in ethanol T=60°C; Hydrolysis; 2 h;
参考文献
Fougerousse, Andre; Gonzalez, Emmanuel; Brouillard, Raymond
Journal of Organic Chemistry, 2000 , vol. 65, # 2 p. 583 - 586
反应条件
[bis(acetoxy)iodo]benzene; potassium hydroxide in methanol T=20°C; 72 h;
参考文献
Sagrera, Gabriel; Seoane, Gustavo
Synthesis, 2010 , # 16 art. no. M06509SS, p. 2776 - 2786
反应条件
in hydrogenchloride; methanol Irradiation;
参考文献
Rao, Sudhakar T.; Singh, Anil Kumar; Trivedi, Girish Kumar
Heterocycles, 1984 , vol. 22, # 6 p. 1377 - 1382
反应条件
hydrogenchloride in ethanol T=20°C; 8 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 16 p. 5375 - 5383
反应条件
pyridine; hydrogenchloride 1. 50 deg C, 15 min 2. 140 deg C, 50 min;
参考文献
Parvez, M.; Ogbeide, O. N.
Phytochemistry (Elsevier), 1990 , vol. 29, # 6 p. 2043 - 2044
反应条件
1: 98 percent / pyridine / 2 h / 20 °C 2: 85 percent / phenyltrimethylammonium tribromide / tetrahydrofuran / 6 h / 20 °C 3: 77 percent / acetonitrile / 48 h / 20 °C 4: NaH / tetrahydrofuran / Heating 5: 357 mg / H2SO4 / acetic acid / 1.5 h / 60 °C 6: 88 percent / NaOH; H2O / ethanol / 2 h / 60 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 2 p. 583 - 586
反应条件
potassium carbonate; Adogen-464 in benzene Ambient temperature; Further byproducts given. Yields of byproduct given;
参考文献
Patonay, Tamas; Patonay-Peli, Erzsebet; Litkei, Gyoergy
Tetrahedron, 1987 , vol. 43, # 8 p. 1827 - 1834
反应条件
1: 85 percent / phenyltrimethylammonium tribromide / tetrahydrofuran / 6 h / 20 °C 2: 77 percent / acetonitrile / 48 h / 20 °C 3: NaH / tetrahydrofuran / Heating 4: 357 mg / H2SO4 / acetic acid / 1.5 h / 60 °C 5: 88 percent / NaOH; H2O / ethanol / 2 h / 60 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 2 p. 583 - 586
