Schneider, B.; Neumann, W. P.
Liebigs Annalen der Chemie, 1967 , vol. 707, p. 7 - 14
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.8, page 63 - 65
AIBN in benzene
heating equimolar amts. of Se-compds. with 5 molpercent of HSnBu3 and 5 molpercent AIBN (80°C, in dark); not isolated, detd. by NMR spectroscopy;
参考文献
Schiesser, Carl H.; Skidmore, Melissa A.
Journal of Organometallic Chemistry, 1998 , vol. 552, # 1-2 p. 145 - 157
hydroquinone; (CO)5W[CNC6H4NO2] in toluene
byproducts: (Bu3Sn)2; alkyne and catalyst with hydroquinone dissolved in abs. toluene, heated for 15 min at 60°C, Bu3SnH added, heated for 12 h at 60°C; solv. removed, chromy over silica gel with pure hexane, then hexane/ethyl acetate/1percent triethylamine, 98-90percent hexane;
参考文献
Braune, Sascha; Kazmaier, Uli
Angewandte Chemie - International Edition, 2003 , vol. 42, # 3 p. 306 - 308
Lambert, Joseph B.; Zhao, Yan; Wu, Hongwei; Tse, Winston C.; Kuhlmann, Barbara
Journal of the American Chemical Society, 1999 , vol. 121, # 21 p. 5001 - 5008
in neat (no solvent)
G.J.M. Van der Kerk, J.G. Noltes and J.G.A. Luijten, J. Appl. Chem., 7 (1957) 356; CH2CHCN and Bu3SnH heated at 80 °C for 4 h; evapd. in vac., flash chromd. (Kieselgel 60, Et2O/light petroleum 5/95);
参考文献
Fleming, Ian; Urch, Christopher J.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 173 - 192
Pereyre, M.; Colin, G.; Valade, J.
Bulletin de la Societe Chimique de France, 1968 , p. 3358 - 3359
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Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.5.2, page 276 - 305
